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GCMS reference standard results, June 5 2002

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Reference standard analysis report for volatile organic compounds using gas chromatography-mass spectrometry on June 5, 2002.

NYC-WTC_000015528–000015535

Folder label: “GCMS X 6/4/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\060402\604REF2.D Vial: 5 Acq On 4 Jun 2002 7:07 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 05 12:10:23 2002 Quant Results File: 060302.RES Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 12:03:00 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 3 6) Fluoroanthene 26.49 202 6649799 16.59 ug/L 99 3 8) Pyrene 27.12 202 6899554 16.87 ug/L 99 39) Butylbenzylphthalate 29.47 149 1802675 17.40 ug/L 99 4 0) Benzo(a)anthracene 30.73 228 4315172 14.97 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.34 149 1861555 17.29 ug/L 98 42) Chrysene 30.82 228 5135098m 16.77 ug/L 44) Di-n-octylphthalate 33.18 149 1575155m 6.63 ug/L 45) Benzo(b)fluoranthene 33.69 252 3144439 14.80 ug/L 98 46) Benzo(k)fluoranthene 33.77 252 4398744 17.24 ug/L 99 47) Benzo(a)pyrene 34.50 252 2217525 10.93 ug/L 98 48) Indeno(l,2,3-cd)pyrene 37.32 27 6 1276392 9.32 ug/L 97 49) Dibenz(a,h)anthracene 37.44 278 1826733 12.14 ug/L 98 50) Benzo(g,h,i)perylene 38.05 276 2273700 14.15 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 604REF2.D 060302.M Wed Jun 05 12:11:00 2002 Page 2

NYC-WTC_000015534

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NYC-WTC_000015534Source: NYC Law Department, mirrored locally

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