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GCMS reference standard results, sample AE11799, May 28, 2002

Machine-extracted title · confidence 100%

Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.

NYC-WTC_000012783–000012793

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\052202\521REF2.D Vial: 5 Acq On : 22 May 2002 5:05 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 28 14:37:23 2002 Quant Results File: 052202.RES

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue May 28 14:25:08 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 3 6) Fluoroanthene 26.49 202 6329723 15.51 ug/L 99 3 8) Pyrene 27.13 202 6650358 19.37 ug/L 99 39) Butylbenzylphthalate 29.48 149 1684438 11.46 ug/L 95 4 0) Benzo(a)anthracene 30.74 228 4127024 15.92 ug/L 100 41) Bis(2-ethylhexyl)phthalate 31.34 149 1660056 8.69 ug/L 99 42) Chrysene 30.83 228 4965155m 16.67 ug/L 44) Di-n-octylphthalate 33.20 149 1477077 6.81 ug/L 99 45) Benzo(b)fluoranthene 33.70 252 3185507 15.94 ug/L 98 46) Benzo(k)fluoranthene 33.78 252 3861250 17.24 ug/L 100 47) Benzo(a)pyrene 34.50 252 2058703 11.51 ug/L 98 48) Indeno(1,2,3-cd)pyrene 37.32 276 1492028 12.52 ug/L 97 49) Dibenz(a,h)anthracene 37.45 278 2021457 15.42 ug/L 98 50) Benzo(g,h,i)perylene 38.06 276 2221318 15.96 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 521REF2.D 052202.M Tue May 28 14:38:01 2002 Page 2

NYC-WTC_000012789

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NYC-WTC_000012789Source: NYC Law Department, mirrored locally

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