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GCMS reference data sample AE11926, May 2002

Machine-extracted title · confidence 90%

Reference data sheet listing concentrations and detection limits for volatile organic compounds used in GCMS analysis on May 29, 2002.

NYC-WTC_000013448–000013453

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\0 52 3 02\522REF1.D Vial: 4 Acq On : 23 May 2002 12:25 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 29 09:39:21 2002 Quant Results File: Q52202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.49 202 7708666 14.28 ug/L 98 3 8) Pyrene 27.13 202 7977495 18.59 ug/L 99 39) Butylbenzylphthalate 29.48 149 2274257 12.38 ug/L 99 4 0) Benzo(a)anthracene 30.74 228 4860442 15.00 ug/L 100 41) Bis(2-ethylhexyl)phthalate 31.35 149 2143865 8.97 ug/L 98 42) Chrysene 30.83 228 5596795m 15.03 ug/L 44) Di-n-octylphthalate 33.19 149 1647417 7.00 ug/L 98 45) Benzo(b)fluoranthene 33.70 252 3230412 14.90 ug/L 99 46) Benzo(k)fluoranthene 33.78 252 3971968 16.35 ug/L 100 4 7) Benzo(a)pyrene 34.50 252 1906587 9.83 ug/L 99 48) Indeno(1,2,3-cd) pyrene 37.32 276 962582 7.44 ug/L # 92 49) Dibenz(a,h)anthracene 37.45 278 1445718 10.16 ug/L 98 50) Benzo(g,h,i)perylene 38.06 276 1600488 10.60 ug/L 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 522REF1.D 052202.M Wed May 29 09:39:57 2002 Page 2

NYC-WTC_000013451

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NYC-WTC_000013451Source: NYC Law Department, mirrored locally

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