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GCMS reference standard results, sample AE11799, May 28, 2002

Machine-extracted title · confidence 100%

Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.

NYC-WTC_000012783–000012793

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\052202\521REFl.D Vial: 4 Acq On : 22 May 2002 4:16 pm Operator: Mclean Sample . : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 28 14:36:28 2002 Quant Results File: 052202.RES

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue May 28 14:25:08 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.50 202 8519902 16.38 ug/L 99 3 8) Pyrene 27.13 202 8867504 19.47 ug/L 99 39) Butylbenzylphthalate 29.48 149 2513007 12.90 ug/L 96 40) Benzo(a)anthracene 30.74 228 5782730 16.82 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.35 149 2651734 10.46 ug/L 98 42) Chrysene 30.84 228 6802658m 17.22 ug/L 44) Di-n-octylphthalate 33.20 149 2477992 8.66 ug/L 100 45) Benzo(b)fluoranthene 33.70 252 4474230 16.97 ug/L 99 46) Benzo(k)fluoranthene 33.78 252 5221851 17.68 ug/L 99 47) Benzo(a)pyrene 34.51 252 2857820 12.12 ug/L 100 48) lndeno(l,2,3-cd)pyrene 37.32 276 1969979 12.53 ug/L 96 49) Dibenz(a,h)anthracene 37.45 278 2618109 15.14 ug/L 100 50) Benzo (g, h, i) perylene 38.06 276 2751330 14.99 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 521REF1.D 052202.M Tue May 28 14:37:14 2002 Page 2

NYC-WTC_000012786

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NYC-WTC_000012786Source: NYC Law Department, mirrored locally

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