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GCMS calibration results for sample AE11417, May 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 23, 2002.

NYC-WTC_000025359–000025362

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\052002\CAL20.D Vial: 2 Acq On : 21 May 2002 12:41 am Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 21 09:01:24 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 20 15:49:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 20659139 23.27 ug/L 99 3 8) Pyrene 27.18 202 19822708 21.22 ug/L 97 39) Butylbenzylphthalate 29.52 149 9350969 22.46 ug/L # 97 40) Benzo(a)anthracene 30.79 228 14553807 19.57 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.38 149 12450744 22.13 ug/L 95 42) Chrysene 30.89 228 15352332 19.93 ug/L 97 44) Di-n-octylphthalate 33.23 149 16709303 20.17 ug/L 98 45) Benzo(b)fluoranthene 33.76 252 16456202 24.22 ug/L 97 46) Benzo(k)fluoranthene 33.83 252 18101092 21.20 ug/L 99 47) Benzo(a)pyrene 34.56 252 15632830 23.05 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.40 276 12387518 26.06 ug/L 99 49) Dibenz(a,h)anthracene 37.52 278 12810231 25.34 ug/L 98 50) Benzo(g,h,i)perylene 38.15 276 13745136 25.90 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL20.D 050102.M Wed May 22 15:55:12 2002 Page 2

NYC-WTC_000025361

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NYC-WTC_000025361Source: NYC Law Department, mirrored locally

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