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GCMS calibration data, June 10 2002

Machine-extracted title · confidence 90%

Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 10, 2002.

NYC-WTC_000015373–000015380

Folder label: “GCMS X 6/3/02 A 6/6/02

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OCR text

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\060602\603REF2.D Vial: 5 Acq On 6 Jun 2002 2:34 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 07 08:21:02 2002 Quant Results File: 060302.RES

Quant Method : C:\MSDCHEM\1\METHODS\060302 .M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu Jun 06 15:03:45 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

3 6) Fluoroanthene 26.49 202 8308280 15.12 ug/L 99 3 8) Pyrene 27.12 202 8433056 17.75 ug/L 99 39) Butylbenzylphthalate 29.48 149 1519472 14.79 ug/L 95 40) Benzo(a)anthracene 30.74 228 4045137 12.07 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.33 149 804232 12.22 ug/L 98 42) Chrysene 30.83 228 4982363m 14.00 ug/L 44) Di-n-octylphthalate 33.18 149 514831 14.89 ug/L 97 45) Benzo(b)fluoranthene 33.70 252 1915848 9.35 ug/L 98 46) Benzo(k)fluoranthene 33.77 252 3803074 15.46 ug/L 98 47) Benzo(a)pyrene 34.50 252 988575 5.05 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.31 276 366920 2.78 ug/L 91 49) Dibenz(a,h)anthracene 37.43 278 698102 4.81 ug/L 89 50) Benzo(g,h,i)perylene 38.05 276 1172910 7.57 ug/L 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 603REF2.D 060302.M Mon Jun 10 10:19:34 2002 Page 2

NYC-WTC_000015379

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NYC-WTC_000015379Source: NYC Law Department, mirrored locally

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