GCMS calibration data, June 10 2002

z Quantitation Report (QT Reviewed) 2 K K O o 3 Data File Acq On C:\MSDCHEM\1\DATA\060602\603REF2.D 6 Jun 2002 2:34 pm Vial: 5 Operator: McLean co — 1 o "0 o Sample 6/3 eh Inst : Instrumen C O o o Mise Multiplr: 1.00 o' o CH MS Integration Params: EVENTS.E "0 o CD 00 Quant Time: Jun 10 10:19 2002 Quant Results File: 060302.RES — o 0 o Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) o Q Title : 508 Modified GC/MS scan C 3 Last Update : Thu Jun 06 15:03:45 2002 CD X Response via : Initial Calibration Abundance TIC: 603REF2.D 3200000 o

3000000 § o I 2 2 2800000 i 5 £ 2600000 $0 2400000 1 2200000 I 2000000 Y N

i 1800000 o2« ! I k to 1600000- o 2

i2 2 0 § I 1400000 2 E la g s8 e O I I : L gi 2 o Eg «2 1200000 yag l Ji I fl 8 § 20 25 | I4 8 8 N

1000000 ok h 2 Q* ]e § 5 Q 2 t t5 s do 8 I & & h 1 I 800000 & 9g £e l 9A § S* s s O 8 X g g 600000 ■s. 5 N* & § | § 2 11 28 1 N c 8 S $2 400000 1f I & 8 v& a

12 c y 00 & 200000

O--T* IT It 1 r l i •! ‘r T rr . । ", " | * —r 11n A UK , — TBI T-T—| Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

603REF2.D 060302.M Mon Jun 10 10:19:35 2002 Page 3