GCMS blank analysis results, June 10 2002

Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\0 6 0 6 0 2\CAL4.D Vial: 2 Acq On 6 Jun 2002 11:00 am Operator: McLean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 6 12:51 2002 Quant Results File: 060302.RES Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 14:47:27 2002 Response via : Initial Calibration Abundance TIC: CAL4.D

2 5000000 § i 4500000

6 o 8« © I4 s © & § 8 2

i I 0 z 8 4000000 8g g £

3500000 2o s _ 0 8g §81) c( £ a

I t§ 11 I 11 "t g82 Il I 88 1582 8o s-g 8 0 5 1c 18% ?a Q

9 S 2

1 i 3000000 th ft SN § N

Is hI h a” s c

2500000: 8i 594 t S I & a I. 8 'c 2

II 3 I 00

&f 88 a &9 0- ( .52 2 8 & 2000000 I S Io e $ N & 2 8 ® 8 y CQ B- £ ® 2

I B8 1500000 N co t & C CD E O 1000000 I F 5 8 1j f& o Q 500000 CXI co ‘t CO t LO o Q 9 0 । . । . i । i । ■ > i i । । ‘I 4 1f — *1 r 11 32.00 I ■n o o o Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 34.00 ' 3600 ' 38.00 o o I 0 o oo CAL4.D 060302.M Thu Jun 06 12:51:11 2002 Page 3 Id > > 7 7