GCMS calibration results for deuterated standards, May 2 2002

2 2 - Quantitation Report (QT Reviewed) - o o 2 Data File C:\MSDCHEM\l\DATA\050102\CAL50.D Vial: 5 co — I o Acq On 1 May 2002 12 : 57 pm Operator: Mclean "0 O C O Sample Inst : Instrumen O O O Mise Multiplr: 1.00 o' MS Integration Params: EVENTS.E "0 o O. Quant Time: May 2 9:42 2002 Quant Results File: 050102.RES — CO 0 o o Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Q C Title 508 Modified GC/MS scan 3 Last Update Thu May 02 09:38:23 2002 CD

Response via Initial Calibration Abundance TIC: CAL50.D 4000000

Q

3500000 §O 2 oCO 2 2 I O 6 z 0) C 0) ■ o 6Co 1 It i 2 0 to f 2 .1 0) 8 g 3000000 g 2 f 3 N

s C

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68 0)

§ 18 e 2o g an 6 o o g N |! 0)

g Si 11 o EK >& 8 n £ ± C 3 c 2 1 2 @ 1 2500000 88 g 5 42 5 & i li e 2 CN § P o 0 C m g 9 & & 88-2 £ C 111 I 8 Hi ifc 8 L- &4a 8 55 3 &ci § g— O Io> 2 J6 a 3 a 3 8 S 3 N

2000000 23 I O

I I H 89 co O 0 6 i i I 1 o

r 0E

I CM CW L

2 g 3 i 1 1500000 CM .2 8 I 2s ca- 0 —

i CM' N 1 5

1000000 II o X 3 500000

o L 1 1 Illi I I I I I I I I I I [ I I I I I I I I I I I I I I I I __ I i LI । i 1 j I i i | | i— 1 > । | 1 I I I I | i I | । | r : i I I I I I I I I 1 >> I I

Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

CAL50.D 050102.M Thu May 02 09:42:37 2002 Page 3