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GCMS calibration results for Method 508, April 2002

Machine-extracted title · confidence 90%

Calibration report for Method 508 GC/MS analysis performed on April 10, 2002, listing internal standards.

NYC-WTC_000039306–000039311

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020408\0408C4.D Vial: 5 Acq On 8 Apr 2002 2:37 pm Operator: McLean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 09 15:10:49 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1... \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 15:05:54 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 31.03 178 19167917 40.76 ug/1 100 35) Anthracene 31.26 178 18861063 41.35 ug/1 100 36) Di-n-butylphthalate 34.00 149 20621307 43.55 ug/1 100 37) Fluoranthene 35.25 202 20208692 41.87 ug/1 100 40) Pyrene 35.86 202 20893917 41.93 ug/1 100 41) Buthylbenzylphthalate 38.11 149 8201078 44.19 ug/1 100 42) Benz(a)anthracene 39.09 228 16474620 42.57 ug/1 100 43) Chrysene 3 9.18 228 15780668 41.59 ug/1 100 44) Bis(2-ethylhexyl)phthalate 39.69 149 9511030 45.04 ug/1 100 46) Di-n-Octyl phthalate 41.20 149 12910761 40.82 ug/1 10 0 47) Benzo(b)fluoranthene 41.55 252 12555875 43.75 ug/1 100 48) Benzo(k)fluoranthene 41.61 252 13362062 40.53 ug/1 100 49) Benzo(a)pyrene 42.19 252 10797068 44.62 ug/1 100 50) Indeno(1,2,3-cd)pyrene 44.37 276 6402435 41.68 ug/1 100 51) Dibenz(a,h)anthracene 44.46 278 6199622 44.81 ug/1 100 52) Benzo(ghi)perylene 44.92 276 6798194 47.41 ug/1 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0408C4.D SCANAPR0902.M Tue Apr 09 15:11:08 2002 Page 2

NYC-WTC_000039310

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NYC-WTC_000039310Source: NYC Law Department, mirrored locally

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