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GCMS calibration results for Method 508, April 2002

Machine-extracted title · confidence 90%

Calibration report for Method 508 GC/MS analysis performed on April 10, 2002, listing internal standards.

NYC-WTC_000039300–000039302

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \MSDCHEM\1\DATA\020408\0408C1.D Vial: 2 Acq On 8 Apr 2002 11:49 am Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 10 14:24:16 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 14:51:40 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 30.99 178 2227868 4.89 ug/1 100 35) Anthracene 31.21 178 2035215 4.60 ug/1 98 36) Di-n-butylphthalate 33.98 149 1833706 4.00 ug/1 100 37) Fluoranthene 35.22 202 2051125 4.39 ug/1 95 40) Pyrene 35.83 202 2169872 4.83 ug/1 95 41) Buthylbenzylphthalate 38.09 149 369485 (2.21 ug/1 87 42) Benz(a)anthracene 39.08 228 1490776 4.27 ug/1 99 43) Chrysene 39.15 228 1625065 4.75 ug/1 100 44) 46) 47) Bis(2-ethylhexyl)phthalate Di-n-Octyl phthalate Benzo(b)fluoranthene 39.68 41.18 41.52 149 149 252 343220 334090 858426 9:80-ug/1 (3.43-ug/1 90 86 95 48) Benzo(k)fluoranthene 41.58 252 1363514 4.74 ug/1 95 49) Benzo(a)pyrene 42.17 252 633453 /3.00 ug/1 94 50) Indeno(1,2,3-cd)pyrene 44.35 276 197362 ug/1 89 51) Dibenz(a,h)anthracene 44.45 278 264593 / 2.19ug/l 92 52) Benzo(ghi)perylene 44.89 276 444096 l 3.55 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0408C1.D SCANAPR0902.M Wed Apr 10 14:25:19 2002 Page 2

NYC-WTC_000039301

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NYC-WTC_000039301Source: NYC Law Department, mirrored locally

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