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GCMS reference results for sample AE06303, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS reference analysis of sample AE06303 conducted on April 9, 2002.

NYC-WTC_000039320–000039322

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\02 040 8\0318REF1.D Vial: 9 Acq On 8 Apr 2002 6:20 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 09 15:08:14 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 15:05:54 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 30.99 178 4687583 8.71 ug/1 99 35) Anthracene 31.22 178 4239225 8.12 ug/1 99 36) Di-n-butylphthalate 33.98 149 5177071 9.55 ug/1 99 37) Fluoranthene 35.23 202 4746746 8.59 ug/1 98 4 0) Pyrene 35.83 202 5025659 8.99 ug/1 97 41) Buthylbenzylphthalate 38.09 149 1662947 7.99 ug/1 95 42) Benz(a)anthracene 39.08 228 3867305 8.91 ug/1 99 43) Chrysene 39.16 228 3959047 9.30 ug/1 99 44) Bis(2-ethylhexyl)phthalate 39.68 149 1907278 8.05 ug/1 97 46) Di-n-Octyl phthalate 41.19 149 1756186 10.44 ug/1 96 47) Benzo(b)fluoranthene 41.52 252 2702900 7.99 ug/1 97 48) Benzo(k)fluoranthene 41.59 252 3241153 8.33 ug/1 96 49) Benzo(a)pyrene 42.17 252 1681685 5.89 ug/1 97 50) Indeno(1,2,3-cd)pyrene 44.35 276 865236 10.06 ug/1 95 51) Dibenz(a,h)anthracene 44.45 278 1190253 7.29 ug/1 96 52) Benzo(ghi)perylene 44.89 276 1392492 8.23 ug/1 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0318REF1.D SCANAPR0902 .M Wed Apr 10 14:38:14 2002 Page 2

NYC-WTC_000039321

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NYC-WTC_000039321Source: NYC Law Department, mirrored locally

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