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GCMS calibration results for Method 508, April 2002

Machine-extracted title · confidence 90%

Calibration report for Method 508 GC/MS analysis performed on April 10, 2002, listing internal standards.

NYC-WTC_000039303–000039305

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020408\0408C2.D Vial: 3 Acq On 8 Apr 2002 12:45 pm Operator: McLean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 10 14:25:26 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 14:51:40 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 30.99 178 4337622 10.05 ug/1 98 35) Anthracene 31.22 178 4109303 9.82 ug/1 100 36) Di-n-butylphthalate 33.98 149 4156042 9.56 ug/1 99 37) Fluoranthene 35.23 202 4277991 9.66 ug/1 97 4 0) Pyrene 35.83 202 4498940 10.03 ug/1 97 41) Buthylbenzylphthalate 38.10 149 1227107 (7.34 ug/1 95 42) Benz(a)anthracene 39.08 228 3298859 9.47 ug/1 99 43) Chrysene 39.16 228 3358822 9.83 ug/1 100 44) Bis(2-ethylhexyl)phthalate 39.69 149 1303132 <6.85 ug/1 93 46) Di-n-Octyl phthalate 41.19 149 1209340 10.20 ug/l 93 47) Benzo(b)fluoranthene 41.53 252 2146163 8.65 ug/1 96 48) Benzo(k)fluoranthene 41.59 252 2736076 9.60 ug/1 96 49) Benzo(a)pyrene 42.17 252 1679499 8.03 ug/1 95 50) Indeno(1,2,3-cd)pyrene 44.35 276 610788 9.91 ug/1 96 51) Dibenz(a,h)anthracene 44.45 278 790244 ( 6.61 ug/1 96 52) Benzo(ghi)perylene 44.89 276 1036855 8.37 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0408C2.D SCANAPR0902.M Wed Apr 10 14:25:59 2002 Page 2

NYC-WTC_000039304

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NYC-WTC_000039304Source: NYC Law Department, mirrored locally

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