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GCMS calibration results for Method 508, April 2002

Machine-extracted title · confidence 90%

Calibration report for Method 508 GC/MS analysis performed on April 10, 2002, listing internal standards.

NYC-WTC_000039315–000039319

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020408\0318REF2.D Vial: 10 Acq On 8 Apr 2002 7:15 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 09 15:08:47 2002 Quant Results File: SCANAPR0902 .R

Quant Method : C:\MSDCHEM\1...\SCANAPR0902. M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 15:05:54 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 30.99 178 4141648 9.40 ug/1 100 35) Anthracene 31.22 178 3722077 8.71 ug/1 100 36) Di-n-butylphthalate 33.98 149 4540940 10.23 ug/1 99 37) Fluoranthene 35.23 202 4116965 9.10 ug/1 96 4 0) Pyrene 35.83 202 4369065 10.01 ug/1 98 41) Buthylbenzylphthalate 38.09 149 1438347 8.85 ug/1 95 42) Benz(a)anthracene 39.08 228 3243694 9.57 ug/1 100 43) Chrysene 39.15 228 3369292 10.14 ug/1 99 44) Bis(2-ethylhexyl)phthalate 39.68 149 1614832 8.73 ug/1 97 46) Di-n-Octyl phthalate 41.19 149 1480406 10.75 ug/1 95 47) Benzo(b)fluoranthene 41.52 252 2253313 8.52 ug/1 97 48) Benzo(k)fluoranthene 41.58 252 2767931 9.11 ug/1 97 49) Benzo(a)pyrene 42.17 252 1433741 6.43 ug/1 94 50) Indeno(1,2,3-cd)pyrene 44.35 276 725395 10.36 ug/1 95 51) Dibenz(a,h)anthracene 44.45 278 1105565 8.67 ug/1 96 52) Benzo(ghi)perylene 44.89 276 1249696 9.46 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0318REF2.D SCANAPR0902 .M Wed Apr 10 14:37:58 2002 Page 2

NYC-WTC_000039318

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NYC-WTC_000039318Source: NYC Law Department, mirrored locally

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