GCMS calibration results for Method 508, April 2002

Z Z Quantitation Report (QT Reviewed) K - o o 3 Data File Acq On C:\MSDCHEM\1\DATA\020408\0408C4.D 8 Apr 2002 2:37 pm Vial: Operator: 5 McLean _s

o "0 1 o Sample Inst : Instrumen C O o Mise o Multiplr: 1.00 o o C MS Integration Params: EVENTS.E “0 O (O C Quant Time: Apr 9 15:10 2002 Quant Results File: SCANAPR0902.RES — 9

U Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) o O C Title : Method 508 GC/MS Scan 3 Last Update : Tue Apr 09 15:05:54 2002 Q

Response via : Initial Calibration Abundance TIC: 0408C4.D

2800000

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8 ! 2000000

1800000

1600000 oil 0)

88 SI8 1 26 92 si if £ 2 o

8 2 2 8 18 2o G £ S' 8 § gi 5l t I I 2 g of a 88 | Sa J Lg s £ 8 o § 2 Oo s CO

i ax I s 3 7. f 8;| l18e d‘ w in A

li & s 8 £

1400000 ! s& 86238 18 2209 o J ( 2 S2 86 - 8 2 o 87 9 & 2 $ c

I 1 1200000 88

I 8 I | 8 1 $2 C. C i § i2 28 I §7 I 1000000' o *2 Q g | M & s c 8 * 1 o 3

8 & 800000 ! 8 6 N T N

600000

400000

200000

0 —........................ JUU UU Jl TT Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 26.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00

0408C4.D SCANAPR0902.M Tue Apr 09 15:11:09 2002 Page 3