GC/MS calibration results, PAH compounds, May 2002

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GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.

NYC-WTC_000045526–000045542

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\MAY0202\9451.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 1-Propanesulfonic acid, methyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.26 8.90 ug/1 803618 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanesulfonic acid, methyl este 138 C4H10O3S 002697-50-9 4 2 Hydrogen azide 43 HN3 007782-79-8 4 3 Methyl tert-butyl disulphide 136 C5H12S2 035166-82-6 3 4 3,8-Nonaqien-2-one, (E) - 138 C9H140 055282-90-1 3 Abundance Scan 133 (6.261 min): 9451.D (-) m/z 43.05 100.00% 43

5000

—— I I ! t | I I I I f I ! I [ I I I I | I I I I 6.00 6.20 6.40 6.60 3644 58 79 93 100107 123 136 I I I I I I I III I I l—I_ I_ 1gu 1 I 1 I I I I I I I I I I I I I m/z 42.05 11.30% 1 ■ ’ ।1111111'' ।' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6820:1-Propanesulfonic acid, methyl ester 43

, . r /— 5000 1 1 1 1 i r 1 r 1 i ' 1 1 ' 1 1 1 1 1 1 1 1 1 1 27 6.00 6.20 6.40 6.60 97 m/z 93.00 4.70% 59 79 107 | 138 1 1 i ' ' 1 1 i ' 1 1 1 i ' ' 1 1 I ' ■ r I I I I ' I I-1 " I I II I I I > 1 i ' ' ' ' i ' ' 1 1 i ' ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #33: Hydrogen azide 43 _. r........ 6.00 6.20 6.40 6.60 5000 15 m/z 136.00 4.64%

1 1 i ■ I ' I | I I I T| * r i f d 1 ■ ■ । ■1 ■ ■ । ■ ■ ■ ■ । ■ 11 ■ ■ ■ t ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ . ■ ।• j ■ ■ ■ ■ । ■ m/z->______ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6400: Methyl tert-butyl disulphide 29 57 6.00 6.20 6.40 6.60 m/z 138.00 4.55% 5000

42 . h 64 73 । — 80 94 । 136 ' ' i ' 1 1 1 i ' ' 111101,11111*10000* —]————— 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60

9451.D GCMS0501.M Fri May 03 08:42:13 2002 Page 1

NYC-WTC_000045531

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