GC/MS calibration table, sample AE09684, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\0425REFl.D Vial: 5 Acq On 7 May 2002 4:06 pm Operator: Nefliu Sample 04/25 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:15:32 2002 Quant Results File: SCAN020507 .RE

Quant Method : C:\MSDCHEM\l\METHQDS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 431843 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1609444 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 854291 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1439232 40.00 ug/1 -0.02 38) Chrysene-dl2 3 9.94 240 1111143 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 699283 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 35596 5.22 ug/1 -0.03 Spiked Amount 10.000 Recovery = 52.20%

Target Compounds Qvalue 2) N-nitrosodimethylamine 4.00 74 55324m 8.04 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 276387 16.54 ug/1 97 4) 1.3-Dichlorbenzene 11.12 146 102967 7.38 ug/1 93 5) 1,4-Dichlorobenzene 11.43 146 113095 7.43 ug/1 96 6) 1,2-Dichlorobenzene 11.96 146 124648 9.43 ug/1 93 7) 2,2'oxybis(1-Chloropropane 12.78 45 454982m 17.05 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 219097 18.34 ug/1 100 9) Hexachloroethane 13.26 119 21491 3.25 ug/1 92 11) Nitrobenzene 13.67 77 322245 16.68 ug/1 98 12) Isophorone 14.78 82 682101 20.27 ug/1 99 13) bis(2-Chloroethoxy) methan 16.02 93 348028 17.41 ug/1 96 14) 1,2,4-Trichlorobenzene 16.39 180 107683 9.33 ug/1 93 15) Naphthalene 16.62 128 622520 15.43 ug/1 99 16) Hexachlorobutadiene 17.40 225 14724 2.20 ug/1 84 18) 2-Chloronaphthalene 21.92 162 334399 16.44 ug/1 98 19) Acenaphthylene 23.75 152 632899 15.95 ug/1 98 20) Dimethyl phthalate 23.84 163 494695 18.64 ug/1 99 21) 2,6-Dinitrotoluene 23.95 77 40781 17.85 ug/1 94 22) Acenaphthene 24.60 153 402255 17.49 ug/1 96 23) 2,4-Dinitrotoluene 25.74 165 98438 16.11 ug/1 95 24) Fluorene 27.01 166 484671 18.32 ug/1 98 25) Diethyl phthalate 27.23 149 547654 20.52 ug/1 96 26) 4-Chlorophenyl-phenylether 27.34 204 216091 16.49 ug/1 99 28) N-Nitrosodiphenylamine 27.94 168 185538 21.52 ug/1 99 29) Azobenzene 28.02 77 679735 16.67 ug/1 98 31) Hexachlorobenzene 29.59 284 127454 16.79 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 123918 16.68 ug/1 93 33) Phenanthrene 31.81 178 678696 18.54 ug/1 98 34) Anthracene 32.04 178 632591 17.06 ug/1 99 35) Di-n-butylphthalate 34.81 149 886436 19.35 ug/1 99

(#) = qualifier out of range (m) = manual integration 0425REF1.D SCAN020507.M Thu May 09 09:16:33 2002 Page 1

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