GCMS reference standard results for sample AE10812, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020521\0517REF3.D Vial: 7 Acq On : 21 May 2002 2:19 pm Operator: Nefliu Sample : 052/17 ref ad Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:18:04 2002 Quant Results File: SCAN020521.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.37 152 502155 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1875524 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 999380 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1726398 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1351058 40.00 ug/1 -0.04 44) Perylene-dl2 43.16 264 769918 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.56 207 266162 33.20 ug/1 -0.04 Spiked Amount 40.000 Recovery 83.00%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.96 74 53959m 6.93 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 312825 16.06 ug/1 95 4) 1.3-Dichlorbenzene 11.11 146 229520 13.91 ug/1 97 5) 1,4-Dichlorobenzene 11.43 146 242260 13.43 ug/1 92 6) 1,2-Dichlorobenzene 11.95 146 240415 15.31 ug/1 97 7) 2,2'oxybis(1-Chloropropane 12.77 45 526883m 17.07 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 237670 16.93 ug/1 99 9) Hexachloroethane 13.26 119 83246 10.54 ug/1 95 11) Nitrobenzene 13.67 77 383388 16.50 ug/1 98 12) Isophorone 14.78 82 744749 18.70 ug/1 98 13) bis(2-Chloroethoxy) methan 16.02 93 389259 16.50 ug/1 99 14) 1,2,4-Trichlorobenzene 16.38 180 207919 14.85 ug/1 99 15) Naphthalene 16.62 128 835299 17.41 ug/1 99 16) Hexachlorobutadiene 17.40 225 92689 11.23 ug/1 94 18) 2-Chloronaphthalene 21.92 162 450964 18.47 ug/1 98 19) Acenaphthylene 23.75 152 746265 15.95 ug/1 99 20) Dimethyl phthalate 23.84 163 563246 17.71 ug/1 98 21) 2,6-Dinitrotoluene 23.96 77 51500 17.64 ug/1 # 78 22) Acenaphthene 24.60 153 487035 17.58 ug/1 98 23) 2,4-Dinitrotoluene 25.74 165 127354 17.30 ug/1 98 24) Fluorene 27.01 166 591349 18.56 ug/1 100 25) Diethyl phthalate 27.22 149 633386 19.69 ug/1 96 26) 4-Chlorophenyl-phenylether 27.35 204 273295 17.22 ug/1 99 28) N-Nitrosodiphenylamine 27.94 168 190941 17.91 ug/1 99 29) Azobenzene 28.02 77 804473 16.47 ug/1 99 31) Hexachlorobenzene 29.60 284 167885 18.02 ug/1 98 32) 4-Bromophenyl-phenylether 29.71 248 156681 16.93 ug/1 93 33) Phenanthrene 31.82 178 798594 17.79 ug/1 99 34) Anthracene 32.05 178 717082 15.84 ug/1 99 35) Di-n-butylphthalate 34.81 149 1043887 18.77 ug/1 100

(#) = qualifier out of range (m) = manual integration 0517REF3.D SCAN020521.M Fri May 24 09:18:36 2002 Page 1

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