GCMS reference data for sample AE10019, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\0426REF2. D Vial: 8 Acq On 7 May 2002 7:03 pm Operator: Nefliu Sample 04/26 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:19:50 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 587510 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 2239446 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.47 164 1190725 40.00 ug/1 -0.01 30) Phenanthrene-diO 31.72 188 2029382 40.00 ug/1 -0.02 38) Chrysene-dl2 39.95 240 1661532 40.00 ug/1 -0.04 44) Perylene-dl2 43.16 264 1087341 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.55 207 75678 7.96 ug/1 -0.03 Spiked Amount 10.000 Recovery = 79.60%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.94 74 49487m 5.28 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 376763 16.58 ug/1 97 4) 1.3-Dichlorbenzene 11.11 146 286808 15.12 ug/1 100 5) 1,4-Dichlorobenzene 11.43 146 296925 14.34 ug/1 99 6) 1,2-Dichlorobenzene 11.95 146 285382 15.87 ug/1 99 7) 2,2'oxybis(1-Chloropropane 12.78 45 649921m 17.90 ug/1 8) N-Nitroso-di-n-propylamine 13.26 43 288129 17.72 ug/1 97 9) Hexachloroethane 13.26 119 112142 12.48 ug/1 98 11) Nitrobenzene 13.67 77 466251 17.34 ug/1 96 12) Isophorone 14.78 82 935814 19.98 ug/1 96 13) bis(2-Chloroethoxy) methan 16.02 93 487809 17.53 ug/1 99 14) 1,2,4-Trichlorobenzene 16.38 180 247500 15.41 ug/1 99 15) Naphthalene 16.62 128 994013 17.71 ug/1 99 16) Hexachlorobutadiene 17.40 225 125793 13.49 ug/1 93 18) 2-Chloronaphthalene 21.93 162 536811 18.94 ug/1 99 19) Acenaphthylene 23.75 152 904835 16.36 ug/1 99 20) Dimethyl phthalate 23.85 163 663012 17.93 ug/1 98 21) 2,6-Dinitrotoluene 23.96 77 58690 18.43 ug/1 92 22) Acenaphthene 24.60 153 580778 18.11 ug/1 99 23) 2,4-Dinitrotoluene 25.73 165 155165 18.22 ug/1 97 24) Fluorene 27.00 166 700524 18.99 ug/1 100 25) Diethyl phthalate 27.23 149 740599 19.91 ug/1 96 26) 4-Chlorophenyl-phenylether 27.34 204 321141 17.58 ug/1 97 28) N-Nitrosodiphenylamine 27.94 168 205245 17.08 ug/1 97 29) Azobenzene 28.03 77 938824 16.52 ug/1 99 31) Hexachlorobenzene 29.60 284 194011 18.12 ug/1 98 32) 4-Bromophenyl-phenylether 29.71 248 185012 17.66 ug/1 92 33) Phenanthrene 31.82 178 950770 18.42 ug/1 98 34) Anthracene 32.05 178 890890 17.04 ug/1 98 35) Di-n-butylphthalate 34.81 149 1238983 19.18 ug/1 99

(#) = qualifier out of range (m) = manual integration 0426REF2.D SCAN020507.M Thu May 09 09:20:27. 2002 Page 1

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