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GCMS reference data for sample AE10019, May 2002

Machine-extracted title · confidence 90%

Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.

NYC-WTC_000044111–000044118

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\0426REF2 .D Vial: 8 Acq On 7 May 2002 7:03 pm Operator: Nefliu Sample 04/26 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:19:50 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 5.08SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.06 202 1060518 18.23 ug/1 98 39) Pyrene 36.66 202 1111770 19.13 ug/1 99 40) Buthylbenzylphthalate 38.93 149 518689 18.55 ug/1 100 41) Benz(a)anthracene 39.92 228 924238 17.94 ug/1 97 42) Chrysene 40.00 228 914551 18.85 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 719725 20.22 ug/1 97 45) Di-n-Octyl phthalate 42.03 149 950455 16.05 ug/1 99 46) Benzo(b)fluoranthene 42.38 252 766303m 18.17 ug/1 47) Benzo(k)fluoranthene 42.44 252 783610 18.16 ug/1 99 4 8) Benzo(a)pyrene 43.02 252 566148 14.01 ug/1 98 49) Indeno(1,2,3-cd)pyrene 45.22 276 436581 14.59 ug/1 98 50) Dibenz(a,h)anthracene 45.32 278 464842 16.39 ug/1 98 51) Benzo(ghi)perylene 45.77 276 487741 17.02 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0426REF2.D SCAN020507.M Thu May 09 09:20:27 2002 Page 2

NYC-WTC_000044117

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NYC-WTC_000044117Source: NYC Law Department, mirrored locally

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