GCMS reference data for sample AE10019, May 2002

2 2 - Quantitation Report (QT Reviewed) - O O

2 Data File Acq On C : \MSDCHEM\ 1 \DATA\ 020507\042 6REF2 . D Vial: 8 co — o 7 May 2002 7:03 pm Operator: Nefliu U I O Sample 04/26 ref Inst : Instrumen C CT O O O Mise Multiplr: 1.00 o' MS Integration Params: Iscint.e U O Quant Time: May 9 9:20 2002 Quant Results File: SCANO20507.RES • 00 0 O Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) o o C Title : Method 508 GC/MS Scan 3 Last Update : Tue May 07 08:04:29 2002 CD Response via : Initial Calibration Abundance TIC: 0426REF2.D

3200000

3000000 N 2800000

2600000

2400000 $ o ! a I€ I o 2200000 i c £ § |g I 2000000 8 8 8 Z s5 re t 9 8 2 2 % s P 1800000 b i it 2

i 2o I P3 1600000 i& a £ 8 E £ 9 i o § co o 1400000 2re 2o 2 I % co “R g 1 §8 —o ga 2 d ED £ re 2 2 3 2 id! f| £ &re o I2 is 6 5® s §o lI 1200000 I I 2 | 5 Bi 1 8 1 sS p MN th 8 ff I g8 ? 1000000 II 8 8 ‘5 g 5 a &8 800000 2 If 81 24 9 g 2 g 3 2 CM

% Gf 2 i #9 80— 8re 600000 I S* s &o x s I N o w X' 5 2 X B& 400000

200000 I Time-> 0t । । । i r । । i i i i । । । । । । r i i i । i t 4.00 6.00 8.00 10.00 12.00 44 14.00 16.00 ........ I 11ttt । p 18.00 20.00 r

22.00 iTi I

24.00 U । I

26.00 | । r ' I ' 1 ' ‘ 14 28.00 30.00 I VA TTT TT 32.00 I I I I I

34.00 I I I I I I

36.00 I

38.00 L —r 40.00 42.00 44.00 46.00

0426REF2.D SCAN020507.M Thu May 09 09:20:28 2002 Page 3