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GC/MS reference analysis results, sample AE09684, May 2002

Machine-extracted title · confidence 90%

Reference gas chromatography-mass spectrometry analysis with manual result entry for sample AE09684, detecting multiple organic contaminants.

NYC-WTC_000043760–000043764

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\020507\0425REF2.D Vial: 6 Acq On 7 May 2002 5:05 pm Operator: Nefliu Sample 04/25 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:16:41 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.05 202 929945 18.84 ug/1 99 3 9) Pyrene 36.66 202 960414 19.77 ug/1 98 4 0) Buthylbenzylphthalate 38.93 149 435980 18.65 ug/1 100 41) Benz(a)anthracene 39.91 228 811286 18.84 ug/1 98 42) Chrysene 40.00 228 802501 19.79 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 556132 18.69 ug/1 97 45) Di-n-Octyl phthalate 42.04 149 772110 15.61 ug/1 99 46) Benzo(b)fluoranthene 42.38 252 650174m 18.45 ug/1 47) Benzo(k)fluoranthene 42.44 252 711054 19.72 ug/1 98 48) Benzo(a)pyrene 43.03 252 539798 15.99 ug/1 95 49) Indeno(1,2,3-cd)pyrene 45.22 276 380063 15.20 ug/1 98 50) Dibenz(a,h)anthracene 45.32 278 405761 17.13 ug/1 98 51) Benzo(ghi)perylene 45.77 276 446242 18.64 ug/1 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0425REF2.D SCAN020507 .M Thu May 09 09:17:20 2002 Page 2

NYC-WTC_000043763

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NYC-WTC_000043763Source: NYC Law Department, mirrored locally

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