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GCMS calibration results, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing calibration results for volatile organic compounds using GCMS methods between May 13 and May 15, 2002.

NYC-WTC_000024437–000024440

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020515\0515C5.D Vial: 2 Acq On 15 May 2002 12:08 pm Operator: Nefliu Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 15 13:17:10 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.11 202 6950633 163.41 ug/1 99 3 9) Pyrene 36.71 202 6515037 166.83 ug/1 99 40) Buthylbenzylphthalate 38.96 149 3329323 177.23 ug/1 96 41) Benz(a)anthracene 39.96 228 5867869 169.52 ug/1 99 42) Chrysene 40.05 228 5380200 165.07 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.54 149 4083718 170.76 ug/1 97 45) Di-n-Octyl phthalate 42.06 149 6700625 191.74 ug/1 98 46) Benzo(b)fluoranthene 42.43 252 4542930 182.52 ug/1 98 47) Benzo(k)fluoranthene 42.50 252 4429209m 173.92 ug/1 48) Benzo(a)pyrene 43.08 252 4268184 178.95 ug/1 100 49) Indeno(1,2,3-cd)pyrene 45.28 276 2846650 161.22 ug/1 100 50) Dibenz(a,h)anthracene 45.38 278 2597566 155.20 ug/1 99 51) Benzo(ghi)perylene 45.85 276 2574395 152.22 ug/1 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0515C5.D SCAN020507.M Thu May 16 14:52:33 2002 Page 2

NYC-WTC_000024439

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NYC-WTC_000024439Source: NYC Law Department, mirrored locally

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