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GCMS reference data for sample AE10019, May 2002

Machine-extracted title · confidence 90%

Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.

NYC-WTC_000044111–000044118

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\0426REFl.D Vial: 7 Acq On 7 May 2002 6:04 pm Operator: Nefliu Sample 04/26 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:18:59 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.06 202 1064228 18.88 ug/1 98 39) Pyrene 36.66 202 1120094 20.06 ug/1 98 40) Buthylbenzylphthalate 38.93 149 535999 19.95 ug/1 97 41) Benz(a)anthracene 39.92 228 924163 18.67 ug/1 99 42) Chrysene 40.00 228 911725 19.56 ug/1 97 43) Bis(2-ethylhexyl)phthalate 40.52 149 729714 21.34 ug/1 99 45) Di-n-Octyl phthalate 42.04 149 977524 16.96 ug/1 98 46) Benzo(b)fluoranthene 42.38 252 760456m 18.52 ug/1 47) Benzo(k)fluoranthene 42.44 252 819420 19.51 ug/1 97 48) Benzo(a)pyrene 43.03 252 592157 15.05 ug/1 98 49) Indeno(1,2,3-cd)pyrene 45.22 276 458073 15.73 ug/1 100 50) Dibenz(a,h)anthracene 45.32 278 498004 18.04 ug/1 98 51) Benzo(ghi)perylene 45.78 276 514971 18.46 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0426REF1.D SCAN020507.M Thu May 09 09:19:43 2002 Page 2

NYC-WTC_000044114

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NYC-WTC_000044114Source: NYC Law Department, mirrored locally

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