GCMS reference data for sample AE10019, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed.)

Data File C:\MSDCHEM\l\DATA\020507\0426REFl.D Vial: 7 Acq On 7 May 2002 6:04 pm Operator: Nefliu Sample 04/26 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:18:59 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 07 08:04:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 567801 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 2184097 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.46 164 1152650 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1966304 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1596459 40.00 ug/1 -0.04 44) Perylene-dl2 43.16 264 1058412 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.55 207 74009 8.04 ug/1 -0.03 Spiked Amount 10.000 Recovery = 80.40%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.94 74 56071m 6.19 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 388972 17.71 ug/1 96 4) 1.3-Dichlorbenzene 11.12 146 288038 15.71 ug/1 96 5) 1,4-Dichlorobenzene 11.43 146 300346 15.01 ug/1 95 6) 1,2-Dichlorobenzene 11.95 146 291674 16.79 ug/1 97 7) 2,2'oxybis(1-Chloropropane 12.78 45 654975m 18.66 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 293624 18.69 ug/1 98 9) Hexachloroethane 13.26 119 103499 11.92 ug/1 96 11) Nitrobenzene 13.67 77 461016 17.58 ug/1 97 12) Isophorone 14.78 82 941776 20.62 ug/1 97 13) bis(2-Chloroethoxy) methan 16.02 93 494709 18.23 ug/1 97 14) 1,2,4-Trichlorobenzene 16.38 180 247497 15.80 ug/1 98 15) Naphthalene 16.62 128 999028 18.25 ug/1 99 16) Hexachlorobutadiene 17.39 225 114970 12.64 ug/1 97 18) 2-Chloronaphthalene 21.93 162 546193 19.90 ug/1 98 19) Acenaphthylene 23.76 152 905487 16.91 ug/1 98 20) Dimethyl phthalate 23.85 163 667328 18.64 ug/1 98 21) 2,6-Dinitrotoluene 23.96 77 61600 19.98 ug/1 92 22) Acenaphthene 24.60 153 586573 18.90 ug/1 97 23) 2,4-Dinitrotoluene 25.74 165 154963 18.80 ug/1 96 24) Fluorene 27.00 166 709996 19.89 ug/1 100 25) Diethyl phthalate 27.23 149 748318 20.79 ug/1 98 26) 4-Chlorophenyl-phenylether 27.35 204 323258 18.28 ug/1 97 28) N-Nitrosodiphenylamine 27.94 168 205216 17.64 ug/1 100 29) Azobenzene 28.03 77 946871m 17.21 ug/1 31) Hexachlorobenzene 29.59 284 198099 19.10 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 188239 18.54 ug/1 92 33) Phenanthrene 31.82 178 962519 19.25 ug/1 100 34) Anthracene 32.. 05 178 891413 17.60 ug/1 99 35) Di-n-butylphthalate 34.81 149 1262347 20.17 ug/1 99 (#) = qualifier out of range (m) = manual integration 0426REF1.D SCAN020507.M Thu May 09 09:19:43 2002 Page 1

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