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GCMS calibration reference data for sample REFA1, April 2002

Machine-extracted title · confidence 90%

Calibration table excerpt from GCMS analysis of sample REFA1 showing surrogate recovery data from April 19, 2002.

NYC-WTC_000043536–000043541

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1802\REFA2.D Vial: 18 Acq On : 19 Apr 2002 4:34 am Operator: Sample : GC/MS SCAN 3/26 Inst : 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 14:57 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 148315 12.69 ug/1 94 34) Phenanthrene 25.66 178 630496 12.00 ug/1 99 35) Anthracene 25.79 178 568518 11.00 ug/1 100 36) Di-n-butylphthalate 27.56 149 755123 11.49 ug/1 99 37) Fluoranthene 29.27 202 615793 11.65 ug/1 96 4 0) Pyrene 29.95 202 633510 11.43 ug/1 95 41) Butylbenzylphthalate 32.08 149 258561 9.54 ug/1 96 42) Benzo(a)anthracene 33.59 228 446182 11.60 ug/1 100 43) Bis(2-ethylhexyl )phthalate 33.86 149 350596 10.11 ug/1 100 44) Chrysene 33.72 228 484748 12.71 ug/1 100 46) Di-n-Octylphthalate 35.60 149 400425 7.53 ug/1 # 99 47) Benzo(b)fluoranthene 36.69 252 399922 11.64 ug/1 97 48) Benzo(k)fluoranthene 36.76 252 407256 12.17 ug/1 98 49) Benzo(a)pyrene 37.67 252 276369 9.76 ug/1 97 50) Indeno(1,2,3-cd)pyrene 41.94 276 282719 9.91 ug/1 97 51) Dibenz(a,h)anthracene 42.03 278 247935 11.40 ug/1 97 52) Benzo(g,h,i)perylene 43.18 276 242968 10.21 ug/1 97

(#) = qualifier out of range (m) = manual integration PFWA n GAMCAA1Q M 1-5 1Q 1E.A.AQ

NYC-WTC_000043540

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NYC-WTC_000043540Source: NYC Law Department, mirrored locally

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