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GCMS calibration quantitation report, Feb 24 2002

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Quantitation report for GCMS calibration standards processed on February 24, 2002.

NYC-WTC_000038262–000038264

Folder label: “GCMS X 2/22/02 A 2/24/02

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Data File : C:\HPCHEM\1\DATA\FEB2102\REFE.D Vial: 71 Acq On : 24 Feb 2002 3:54 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 25 8:17 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 87610 " 6.62 ug/1 # 88 31) 4-Bromophenyl-phenylether 24.39 248 57011 6.66 ug/1 96 32) Hexachlorobenzene 24.82 284 66350 6.62 ug/1 99 3 3) Phenanthrene 25.80 178 327811 8.03 ug/1 99 3 4) Anthracene 25.93 178 315824 7.89 ug/1 99 35) Di-n-butylphthalate 27.70 149 436143 7.64 ug/1 99 36) Fluoranthene 29.43 202 323197 7.93 ug/1 # 91 3 9) Pyrene 30.10 202 338451 7.89 ug/1 # 85 40) Butylbenzylphthalate 32.23 149 162417 6.84 ug/1 96 41) Benzo(a)anthracene 33.75 228 254132 8.11 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.01 149 216641 6.75 ug/1 96 43) Chrysene 33.87 228 271275 8.79 ug/1 99 45) Di-n-Octylphthalate 35.75 149 279754 5.27 ug/1 # 97 46) Benzo(b)fluoranthene 36.87 252 205683 6.87 ug/1 # 95 47) Benzo(k)fluoranthene 36.94 252 256850 8.54 ug/1 # 97 48) Benzo(a)pyrene 37.88 252 182247 7.34 ug/1 # 95 4 9) Indeno(1,2,3-cd)pyrene 42.28' 276 192015 8.48 ug/1 # 92 5 0) Dibenz(a,h)anthracene 42.36 278 162937 9.41 ug/1 # 93 51) Benzo(g,h,i)perylene 43.54 276 167163 9.16 ug/1 # 94

(#) = qualifier out of range (m) = manual integration REFE.D GCMS0208.M Wed Mar 13 11:09:16 2002 Page 2

NYC-WTC_000038263

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NYC-WTC_000038263Source: NYC Law Department, mirrored locally

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