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GCMS calibration table data, Nov 2001

Machine-extracted title · confidence 100%

Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.

NYC-WTC_000033723–000033725

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\ 1 \DATA\NOV2 6 01 \CAL2 5 . D Vial: 4 Acq On : 26 Nov 2001 1:36 pm Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 15:04 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue

3 3) Acenaphthylene 20.11 152 3441379 24.92 ug/1 100 3 4) Acenaphthene 20.68 153 2453518 24.85 ug/1 100 35) 2,4-Dinitrophenol 20.88 184 230749 21.46 ug/1 100 36) 4-Nitrophenol 21.16 65 279494 24.85 ug/1 100 37) 2,4-Dinitrotoluene 21.34 165 849080 24.70 ug/1 100 38) Diethylphthalate 22.10 149 2615580 24.70 ug/1 100 39) 4-Chlorophenyl-phenylether 22.22 204 1167768 25.26 ug/1 100 40) Fluorene 22.19 166 2566718 25.33 ug/1 100 41) Azobenzen/ 1,2-Diphenylhyd 22.69 77 2680901 24.50 ug/L 100 43) 4,6-Dinitro-2-methylphenol 22.55 198 426211 24.09 ug/1 100 44) N-Nitrosodiphenylamine 22.62 168 1083405 24.39 ug/1 100 45) 4-Bromophenyl-phenylether 23.68 248 617135 25.08 ug/1 100 46) Hexachlorobenzene 24.10 284 680498 25.15 ug/1 100 47) Pentachlorophenol 24.66 266 321995 25.15 ug/1 100 48) Phenanthrene 25.07 178 3322260 25.08 ug/1 99 49) Anthracene 25.20 178 3350978 25.38 ug/1 100 50) Di-n-butylphthalate 27.01 149 4469724 25.35 ug/1 100 51) Fluoranthene 28.68 202 3235102 25.30 ug/1 100 54) Pyrene 29.34 202 3310786 24.83 ug/1 100 55) Butylbenzylphthalate 31.52 149 1735871 24.93 ug/1 100 56) Benzo(a)anthracene 32.98 228 2302644 25.02 ug/1 100 57) Bis(2-ethylhexyl)phthalate 33.31 149 2346305 24.94 ug/1 100 58) Chrysene 33.11 228 2257807 25.01 ug/1 100 60) Di-n-Octylphthalate 35.05 149 3548135 24.96 ug/1 100 61) Benzo(b)fluoranthene 36.06 252 1965927 24.43 ug/1 100 62) Benzo(k)fluoranthene 36.13 252 2144911 25.97 ug/1 100 63) Benzo(a)pyrene 36.96 252 1735052 24.80 ug/1 100 64) Indeno(l,2,3-cd)pyrene 40.81 276 1685950 24.10 ug/1 100 65) Dibenz(a,h)anthracene 40.88 278 1315973 24.02 ug/1 100 66) Benzo(g,h,i)perylene 41.91 276 1432518 23.96 ug/1 100

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Wed Nov 28 15:05:10 2001 Page 2

NYC-WTC_000033724

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NYC-WTC_000033724Source: NYC Law Department, mirrored locally

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