GCMS calibration table data, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2601\CAL25.D Vial: 4 Acq On : 26 Nov 2001 1:36 pm Operator; 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 15:04 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 922980 20.00 ug/1 0.00 15) Naphthalene-d8 15.31 136 3555516 20.00 ug/1 0.00 26) Acenaphthene-diO 20.58 164 1722223 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 2501577 20.00 ug/1 0.01 53) Chrysene-dl2 33.04 240 1544686 20.00 ug/1 0.00 59) Perylene-dl2 37.12 264 1069709 20.00 ug/1 0.00

System Monitoring Compounds 52) 2,4-DDD 29.90 235 11226 0.38 ug/mL -0.17 Spiked Amount 5.000 Recovery = 7.60%

Target Compounds Qvalue 2) Pyridine 5.37 79 1562622m 23.78 ug/1 3) N-nitroso-dimethyl amine 5.43 74 1008105 24.83 ug/1 100 4) Phenol 10.97 94 2025515 24.89 ug/1 100 5) bis(2-Chloroethyl)ether 11.13 93 1546323 24.27 ug/1 100 6) 2-Chlorophenol 11.24 128 1511097 24.55 ug/1 100 7) 1,3-Dichlorobenzene 11.60 146 1658817 24.71 ug/1 100 8) 1,4-Dichlorobenzene 11.75 146 1681205 24.77 ug/1 100 9) 1,2-Dichlorobenzene 12.25 146 1545759 24.69 ug/1 100 10) 2-Methylphenol 12.55 108 1411231 25.34 ug/1 100 11) 2,2'-oxybis(1-Chloropropan 12.59 45 2024977 24.96 ug/1 100 12) 3&4-Methylphenol 12.97 108 1451644 25.44 ug/1 100 13) N-Nitroso-di-n-propylamine 12.99 70 902898 24.88 ug/1 100 14) Hexachloroethane 13.09 117 611680 24.78 ug/1 100 16) Nitrobenzene 13.38 77 1364398 24.62 ug/1 100 17) Isophorone 14.03 82 2634961 24.68 ug/1 100 18) 2-Nitrophenol 14.29 139 849483 24.44 ug/1 100 19) 2,4-Dimethylphenol 14.45 107 1313801 25.19 ug/1 100 20) bis(2-Chloroethoxy)methane 14.71 93 1775334 24.75 ug/1 100 21) 2,4-Dichlorophenol 14.97 162 1170634 25.44 ug/1 100 22) 1,2,4-Trichlorobenzene 15.20 180 1284635 24.88 ug/1 100 23) Naphthalene 15.36 128 4281567 25.20 ug/1 100 24) Hexachlorobutadiene 15.90 225 631140 25.09 ug/1 100 25) 4-Chloro-3-methylphenol 17.11 107 1164206 25.34 ug/1 100 2 7) Hexachlorocyclopentadiene 18.08 237 287779 23.19 ug/1 100 28) 2,4,6-Trichlorophenol 18.37 196 744759 25.10 ug/1 100 29) 2,4,5-Trichlorophenol 18 .48 196 817511 25.11 ug/1 100 30) 2-Chloronaphthalene 18.85 162 2435397 24.79 ug/1 100 31) Dimethylphthalate 19.96 163 2818105 24.62 ug/1 100 32) 2,6-Dinitrotoluene 20.17 165 667674m 24.69 ug/1

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Wed Nov 28 15:05:07 2001 Page 1

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