GC/MS quantitation report for calibration mix 5, Oct 2001

NYC 9/11 Public Portal Document

Quantitation RgRort (QT Reviewed) Data File C;\HPCHEM\1\DATA\OCT090 CALS.D Vial: 3 Acq On 9 Oct 2001 3:19 pm Operator; 209 GALOS Sample calib mix 5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 11 9:41 2001 Quant Results File: NP09110i.RE; Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via ; Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.78 152 377372 20.00 ug/1 -0.13 19) Naphthalene-d8 15.39 136 1458098 20.00 ug/1 -0.14 31) Acenaphthene-dlO 20.66 164 668540 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.08 188 937790 20.00 ug/1 -0.15 59) Chrysene-dl2 33.12 240 553315 20.00 ug/1 -0.15 68) Perylene-dl2 37.23 264 366236 20.00 ug/1 -0.19

System Monitoring Compounds 4) 2-Fluorophenol 8.63 112 1972837 71.34 ug/1 Spiked Amount 75.000 Recovery 95.12% 5) Phenol-d5 11.03 99 2348639 77.47 ug/1 Spiked Amount 75.000 Recovery = 103.29% 6) 2-Chlorophenol-d4 11.28 132 2043459 71.67 ug/1 3 Spiked Amount 75.000 Recovery 95.56% 7) 1,2-Dichlorobenzene-d4 12.29 152 875453 47.56 ug/1 Spiked Amount 50.000 Recovery 95.12% 20) Nitrobenzene-d5 13.41 82 1256145 !50.91 ug/1 -0.14 Spiked Amount 50.000 Recovery = 101.82% 32) 2-Fluorobiphenyl 18.67 172 2150974 47.63 ug/1 Spiked Amount 50.000 Recovery = ■ 95.26% 33) 2,4,6-Tribromophenol 23.09 330 379691 I64.58 ug/1 -0/.15 Spiked Amount 62) Terphenyl-dl4 Spiked Amount 75.000 50.000 30.00 244 Recovery 1693953 Recovery 86.11% !50.79 ug/1 = 101.58% -L Target Compounds ' Qvalue 2) Pyridine 5.48 79 145240m 4.75 ug/1 3) N-nitroso-dimethyl amine 5.50 74 94939 5.21 ug/1 95 8) Phenol 11.06 94 189375 5.45 ug/1 99 9) bis(2-Chloroethyl)ether 11.20 93 148835 5.61 ug/1 97 10) 2-Chlorophenol 11.32 128 140974 5.24 ug/1 94 11) 1,3-Dichlorobenzene 11.67 146 151060 5.18 ug/1 99 12) 1,4-Dichlorobenzene 11.82 146 154500 5.26 ug/1' 99 13) 1,2-Dichlorobenzene 12.33 146 141668 5.21 ug/1 # 97 14) 2-Methylphenol 12.63 108 128006 5.49 ug/1 99 15). 2,2 '-oxybis (1-Chloropropan 12.66 45 203530 5.43 ug/1 # 84 16) 3&4-Methylphenol 13.04 108 128736 5.41 ug/1 98 17) N-Nitroso-di-n-propylamine 13.05 70 88764 5.32 ug/1 95 18) Hexachloroethane 13.17 117 49397 4.99 ug/1 99 21) Nitrobenzene 13.45 77 133575 5.53 ug/1 100 22) Isophorone 14.09 82 242094 5.24 ug/1 98 (#) = qualifier out of range (m) = manual integration CAL5.D NP091101.M Thu Oct 11 11:00:59 2001 Page 1

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