GC/MS quantitation report for calibration mix 5, Oct 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT0901\CAL5.D Vial: 3 Acq On : 9 Oct 2001 3:19 pm Operator: 209 GALOS Sample : calib mix 5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 11 9:41 2001 Quant Results File: NP091101.RES' . Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 14.36 139 76681 4.98 ug/1 99 24) 2,4-Dimethylphenol 14.53 107 107592 5.22 ug/l 98 25) bis(2-Chloroethoxy)methane 14.78 93 159137 5.35 ug/1 100 26) 2,4-Dichlorophenol 15.06 162 98421 5.09 ug/1 97 27) 1,2,4-Trichlorobenzene 15.27 180 106252 5.32 ug/1 99 28) Naphthalene 15.43 128 392840 5.47 ug/1 # 80 29) Hexachlorobutadiene 15.99 225 51600 5.16 ug/1 96 30) 4-Chloro-3-methylphenol 17.20 107 98196 5.25 ug/1 97 34) Hexachlorocyclopentadiene 18.17 237 6616 —‘1.24 ug/1 96 35) 2,4,6-Trichlorophenol 18.45 196 60279 5.05 ug/1 100 36) 2,4,5-Trichlorophenol 18.57 196 64359 4.92 ug/1 98 37) 2-Chloronaphthalene 18.93 162 211192 5.24 ug/1 100 38) Dimethylphthalate 20.03 163 237825 5.19 ug/1 100 39) 2,6-Dinitrotoluene 20.24 165 52938 4.84 ug/1 94 4 0) Acenaphthylene 20.19 152 310727 5.16 ug/1 99 41) Acenaphthene 20.75 153 222864 5.41 ug/1 99 42) 2,4-Dinitrophenol 20.96 184 4469 0.96 ug/1 91 43) 4-Nitrophenol 21.26 65 22717 4.11 ug/1 93 44) 2,4-Dinitrotoluene 21.40 165 66620 4.75 ug/1 93 45) Diethylphthalate 22.16 149 235384 5.24 ug/1 99 46) 4-Chlorophenyl-phenylether 22.30 204 101102 5.49 ug/1 98 47) Fluorene 22.26 166 225567 5.41 ug/1 99 48) Azobenzen/ 1,2-Diphenylhyd 22.77 77 260088 5.37 ug/L 98 50) 4,6-Dinitro-2-methylphenol 22.62 198 18796 ^.2.94 ug/1 97 51) N-Nitrosodiphenylamine 22.70 168 96539 5.45 ug/1 99 52) 4-Bromophenyl-phenylether 23.76 248 52033 5.08 ug/1 92 53) Hexachlorobenzene 24.18 284 58634 5.38 ug/1 98' 54) Pentachlorophenol 24.75 266 15839 -- 2.71 ug/1 91 55) Phenanthrene 25.15 178 287958 5.49 ug/1 99 56) Anthracene 25.28 178 276963 5.26 ug/1 99 57) Di-n-butylphthalate 27.08 149 399311 5.31 ug/1 100 5 8) Fluoranthene 28.76 202 263731 5.08 ug/1 99 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 29.43 202 268987 5.83 ug/1 99 64) Butylbenzylphthalate 31.59 149 152091 5.71 ug/1 95 65) Benzo(a)anthracene 33.07 228 175124 5.06 ug/1 98 66) Bis(2-ethylhexyl)phthalate 33.39 149 216021 5.90 ug/1 100 67) Chrysene 33.19 228 174443 5.26 ug/1 99 69) Di-n-Octylphthalate 35.13 149 ■ 319648 5.55 ug/1 98 70) Benzo(b)fluoranthene 36.15 252 156464 5.29 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL5.D NP091101.M Thu Oct 11 11:01:03 2001 Page 2

NYC-WTC_000088045