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GCMS reference analysis results for sample AD28143, Nov 2001

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Laboratory report listing quantitative results and detection limits for various organic compounds in a GCMS reference sample analyzed on November 28, 2001.

NYC-WTC_000033907–000033910

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\NOV2601\CAL10.D Vial: 3 Acq On : 26 Nov 2001 12:37 pm Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 8:43 2001 Quant Results File: NP103001.RES

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue

17) N-Nitroso-di-n-propylamine 12.97 70 362245 9.70 ug/1 98 18) Hexachloroethane 13.08 117 249125 9.75 ug/1 99 21) Nitrobenzene 13.37 77 556920 9.86 ug/1 98 22) Isophorone 14.02 82 1074963 9.98 ug/1 99 23) 2-Nitrophenol 14.29 139 359186 9.86 ug/1 97 24) 2,4-Dimethylphenol 14.44 107 540659 9.55 ug/1 95 25) bis(2-Chloroethoxy)methane 14.71 93 728622 10.23 ug/1 99 26) 2,4-Dichlorophenol 14.97 162 471506 9.91 ug/1 99 27) 1,2,4-Trichlorobenzene 15.20 180 529027 10.61 ug/1 98 28) Naphthalene 15.36 12 8 1781622 10.39 ug/1 99 29) Hexachlorobutadiene 15.90 225 258333 10.70 ug/1 99 30) 4-Chloro-3-methylphenol 17.11 107 467316 9.35 ug/1 95 34) Hexachlorocyclopentadiene 18.09 237 79517 8.46 ug/1 98 35) 2,4,6-Trichlorophenol 18.36 196 294262 9.31 ug/1 98 36) 2,4,5-Trichlorophenol 18.47 196 315477 9.10 ug/1 100 37) 2-Chloronaphthalene 18.84 162 993723 10.12 ug/1 99 38) Dimethylphthalate 19.95 163 1153268 10.02 ug/1 99 39) 2,6-Dinitrotoluene 20.16 165 263493 9.51 ug/1 99 40) Acenaphthylene 20.11 152 1399006 10.00 ug/1 99 41) Acenaphthene 20.67 153 1026435 10.26 ug/1 100 42) 2,4-Dinitrophenol 20.87 184 54091 4.60 ug/1 96 43) 4-Nitrophenol 21.15 65 101061 7.98 ug/1 87 44) 2,4-Dinitrotoluene 21.33 165 330242 9.44 ug/1 92 45) Diethylphthalate 22.09 149 1076470 9.90 ug/1 98 46) 4-Chlorophenyl-phenylether 22.22 204 487148 10.66 ug/1 94 47) Fluorene 22.18 166 1077788 10.60 ug/1 100 48) Azobenzen/ 1,2-Diphenylhyd 22.68 77 1107472 9.89 ug/L 96 50) 4,6-Dinitro-2-methylphenol 22.54 198 137278 7.91 ug/1 97 51) N-Nitrosodiphenylamine 22.61 168 451218 12.23 ug/1 97 52) 4-Bromophenyl-phenylether 23.68 248 248323 10.37 ug/1 97 53) Hexachlorobenzene 24.09 284 279421 11.17 ug/1 95 54) Pentachlorophenol 24.66 266 106080 7.68 ug/1 99 5 5) Phenanthrene 25.07 178 1373022 10.45 ug/1 99 56) Ant hr acene 25.19 178 1355421 10.30 ug/1 100 57) Di-n-butylphthalate 27.00 149 1816949 10.10 ug/1 99 58) Fluoranthene 28.67 202 1309678 10.43 ug/1 99 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS1126.M Wed Jan 09 13:15:51 2002 Page 2

NYC-WTC_000033908

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