GCMS reference analysis results for sample AD28143, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\INSTRU~1\209\DATA\NOV2601\CAL10.D Vial: 3 Acq On : 26 Nov 2001 12:37 pm Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 27 8:43 2001 Quant Results File: NP103001.RES

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.70 152 892073 20.00 ug/1 -0.03 19) Naphthalene-d8 15.31 136 3414365 20.00 ug/1 -0.03 31) Acenaphthene-diO 20.58 164 1672479 20.00 ug/1 -0.03 49) Phenanthrene-diO 24.99 188 2384723 20.00 ug/1 -0.04 59) Chrysene-dl2 33.03 240 1494871 20.00 ug/1 -0.03 68) Perylene-dl2 37.12 264 1116792 20.00 ug/1 -0.04

System Monitoring Compounds 4) 2-Fluorophenol 8.55 112 4346374 165.83 ug/1 -0.03 Spiked Amount 75.000 Recovery 87.77% 5) Phenol-d5 10.95 99 5235833 ।68.94 ug/1 -0.04 Spiked Amount 75.000 Recovery = 91.92% 6) 2-Chlorophenol-d4 11.20 132 4310193 66.79 ug/1 -0.03 Spiked Amount 75.000 Recovery = 89.05% 7) 1,2-Dichlorobenzene-d4 12.21 152 1912749 47.17 ug/1 -0.03 Spiked Amount 50.000 Recovery = 94.34% 20) Nitrobenzene-d5 13.32 82 2638768 45.13 ug/1 -0.03 Spiked Amount 50.000 Recovery = 90.26% 32) 2-Fluorobiphenyl 18.58 172 5001777 46.30 ug/1 -0.03 Spiked Amount 50.000 Recovery = 92.60% 33) 2,4,6-Tribromophenol 23.00 330 864232 75.28 ug/1 -0.03 Spiked Amount 75.000 Recovery = 100.37% 62) Terphenyl-dl4 29.91 244 3836889 42.85 ug/1 -0.03 Spiked Amount 50.000 Recovery = 85.70%

Target Compounds Qvalue 2) Pyridine 5.39 79 606920m 9.30 ug/1 3) N-nitroso-dimethyl amine 5.44 74 401053 9.78 ug/1 99 8) Phenol 10.96 94 852925 9.01 ug/1 99 9) bis(2-Chloroethyl)ether 11.13 93 670842 9.88 ug/1 96 10) 2-Chlorophenol 11.24 128 627554 9.36 ug/1 97 11) 1,3-Dichlorobenzene 11.60 146 681265 10.02 ug/1 100 12) 1,4-Dichlorobenzene 11.74 146 695474 10.14 ug/1 99 13) 1,2-Dichlorobenzene 12.25 146 639573 10.09 ug/1 98 14) 2-Methylphenol 12.54 108 576229 9.52 ug/1 99 15) 2,2'-oxybis(1-Chloropropan 12.59 45 841107 10.16 ug/1 # 94 16) 3&4-Methylphenol 12.96 108 591480 9.55 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS1126.M Wed Jan 09 13:15:43 2002 Page 1

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