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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

'Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\23799,D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : . Multiplr: 1,00 MS Integration Params: RTEINT.P Quant Time: Oct 31 11:57 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901,M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901'

Compound R,T, Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. .26) 2,4-Dichlorophenol 0.00 162 .0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 15.37 128 231 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylpheriol 0.00 107 .0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D, 36) 2,4,5-Trichlorophenol 0.00 196 0 N,D, 37) 2-Chl6ronaphthalene 0.00 162 0 N,D, 38) Dimethylphthalate 0.00 163 0 N,D, 39) 2,6-Dinitrotoluene 0.00 165 0 N,D. d 40) Acenaphthylene 0.00 152 0 . N,D, 41) Acenaphthene 0.00 153 0 N,D, 42) 2,4-Dinitrophenol 0.00 184 0 N,D, 43) 4-Nitrophenol 0.00 65 0 N,D, 44) 2,4-Dinitrotoluene 21.13 165 290 . N,D, 45) Diethylphthalate 22.09 149 442 N,D, 46) 4-Chlorophenyl-phenylether 0.00 204 0 N,D, 47) Fluorene 0.00 166 0 .N,D, 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D, 50) 4,6-Dinitro-2-methylphenol 0.00 198 O’ . N,D, ---- 5 T) - N-Nitrosodiphenylamine“ 0T00“r68 —o~? : 'NTD'/ 52) 4-Bromophenyl-phenylether 0.00 248 0 N,D, 53) Hexachlorobenzene 0.00 284 0. N,D, 54) Pentachlorophenol 0.00 266 0 N,D, 5 5) Phenanthrene 25.03 178 913 N,D, 56) Anthracene 25.03 178 913 N.D, _—57) Di-n-butylphthalate—----- 27,03—149— 5871— ~-N,D,-- 5 8) Fluoranthene 0,00 202 .0 N.D. 60) 3,3'-Dichlorobenzidine - 0,00 252 ■ - - 0 N.D. 7—7—7-BenzidineZ7'-~ ~ ' 7TO7:OOT7'T8:4T/~"^’==^0'“ - N ..D... 6'3')’ Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 31.53 149 229 N.D. 65) Benzo(a)anthracene 33.07 228 - 6133 N.D. ---- 66 )~Bis*(;27eeKylhexyl') pHtKalaEe 3'3'733' 149 8846 . N,D, 67) Chrysene 33.13 228 1171 . N,D, 69) Di-n-Octylphthalate 35.08 149 8579 ■ ■ N,D, 70) Benzo(b)fluoranthene 36.14 252 8576 ■ N,D, (#) = qualifier out of range (m) = manual integration 23799,D NP101901,M Wed Oct 31 11:58:37 2001 Page 2

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