GCMS calibration results for volatile organics, Dec 2001

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\DEC1901\CAL25.D Vial: 2 Acq On 19 Dec 2001 10:40 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 19 11:28 2001 Quant Results File: NP091101.RES

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue

17) N-Nitroso-di-n-propylamine 12.96 70 1243481 25.86 ug/1 91 18) Hexachloroethane 13.07 117 763346 26.74 ug/1 98 21) Nitrobenzene 13.36 77 1878795 27.18 ug/1 93 22) Isophorone 14.01 82 3485675 26.34 ug/1 97 23) 2-Nitrophenol 14.27 139 953511 21.61 ug/1 # 84 24) 2,4-Dimethylphenol 14.42 107 1543062 26.14 ug/1 91 25) bis(2-Chloroethoxy)methane 14.69 93 2275544 26.69 ug/1 99 26) 2,4-Dichlorophenol 14.95 162 1367017 24.69 ug/1 97 27) 1,2,4-Trichlorobenzene 15.18 180 1512065 26.44 ug/1 98 2 8) Naphthalene 15.34 128 5112438 24.84 ug/1 99 29) Hexachlorobutadiene 15.88 225 768563 26.86 ug/1 99 30) 4-Chloro-3-methylphenol 17.09 107 1497951 27.94 ug/1 88 34) Hexachlorocyclopentadiene 18.07 237 258630 C 15.69) ug/1 100 35) 2,4,6-Trichlorophenol 18.34 196 832410 22.64 ug/1 99 36) 2,4,5-Trichlorophenol 18.45 196 940809 23.34 ug/1 99 37) 2-Chloronaphthalene 18.83 162 2914819 23.45 ug/1 98 38) Dimethylphthalate 19.95 163 3391584 24.01 ug/1 99 39) 2,6-Dinitrotoluene 20.16 165 804689 23.87 ug/1 # 90 40) Acenaphthylene 20.09 152 4145326 22.32 ug/1 99 41) Acenaphthene 20.66 153 2964668 23.36 ug/l 99 42) 2,4-Dinitrophenol 20.87 184 153701 10.66 ug/1 # 85 43) 4-Nitrophenol 21.14 65 373946 21.97 ug/1 # 82 44) 2,4-Dinitrotoluene 21.33 165 1027519 23.78 ug/1 94 45) Diethylphthalate 22.08 149 3288826 23.77 ug/1 99 46) 4-Chlorophenyl-phenylether 22.21 204 1419938 25.02 ug/1 96 4 7) Fluorene 22.17 166 3067870 23.89 ug/1 99 4 8) Azobenzen/ 1,2-Diphenylhyd 22.68 77 3880134 126.01 ug/L 99 50) 4,6-Dinitro-2-methylphenol 22.54 198 408522 119.53 uq/I # 85 51) N-Nitrosodiphenylamine 22.61 168 1368798 23.61 ug/1 95 52) 4-Bromophenyl-phenylether 23.66 248 757807 22.62 ug/1 # 93 5 3) Hexachiorobenzene 24.08 284 870544 24.42 ug/1 98 54) Pentachlorophenol 24.65 266 333362 17.44 ug/l 99 5 5) Phenanthrene 25.06 178 4095709 23.88 ug/1 99 56) Anthracene 25.18 178 4067164 23.62 ug/1 99 57) Di-n-butylphthalate 26.99 149 5574921 22.66 ug/1 # 99 58) Fluoranthene 28.66 202 4117683 24.23 ug/1 99 60) 3,3’-Dichlorobenzidine 0.00 252 0

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Thu Jan 03 09:58:51 2002 Page 2

NYC-WTC_000016691