GC/MS calibration data for TCLP method, Oct 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1101\C7VL10.D Vial: 2 Acq On : 11 Oct 2001 10:24 am Operator: 209 GALOS Sample : mix Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 11 12:12 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 14.36 139 185024 10.70 ug/1 96 24) 2,4-Dimethylphenol 14.53 107 225037 9.72 ug/l 99 25) bis(2-Chloroethoxy)methane 14.78 93 347710 10.40 ug/1 100 26) 2,4-Dichlorophenol 15.05 162 231999 10.69 ug/1 99 27) 1,2,4-Trichlorobenzene 15.27 180 233568 10.42 ug/1 100 28) Naphthalene 15.44 128 866984 10.75 ug/1 # 80 29) Hexachlo'robutadiene 15.98 225 116025 10.34 ug/1 96 30) 4-Chloro-3-methylphenol 17.19 107 228477 10.87 ug/1 100 34) Hexachlorocyclopentadiene 18.16 237 36754 6.10 ug/1 97 35) 2,4,6-Trichlorophenol 18.45 196 140870 10.48 ug/1 99 36) 2,4,5-Trichlorophenol 18.57 196 154859 10.51 ug/1 99 37) 2-Chloronaphthalene 18.92 162 469735 10.34 ug/1 100 38) Dimethylphthalate 20.04 163 525453 10.17 ug/1 99 39) 2,6-Dinitrotoluene 20.24 165 123168 9.99 ug/1 94 40) Acenaphthylene 20.19 152 704911 10.38 ug/1 100 41) Acenaphthene 20.75 153 485856 10.47 ug/1 99 42) 2,4-Dinitrophenol 20.96 184 23002 4.36 ug/1 95 43) 4-Nitrophenol 21.26 65 59543 9.57 ug/1 ' 98 44) 2,4-Dinitrotoluene 21.40 165 158478 10.03 ug/1 97 45) Diethylphthalate 22.17 149 517413 10.23 ug/1 99 46) 4-Chlorophenyl-phenylether 22.30 204 221337 10.67 ug/1 98 47) Fluorene 22.27 166 502546 10.70 ug/1 100 48) Azobenzen/ 1,2-Diphenylhyd 22.77 77 579755 10.63 ug/L 99 50) 4,6-Dinitro-2-methylphenol 22.62 198 59932 8.26 ug/1 99 51) N-Nitrosodiphenylamine 22.70 168 226021 11.24 ug/1 99 52) 4-Bromophenyl-phenylether 23.76 248 119282 10.26 ug/1 94 53) Hexachlorobenzene 24.18 284 130295 10.53 ug/1 98 54) Pentachlorophenol 24.75 266 54193 8.17 ug/1 96 5 5) Phenanthrene 25.15 178 634041 10.66 ug/1 100 56) TVnthracene 25.29 178 631426 10.57 ug/1 100 57) Di-n-butylphthalate 27.09 149 872924 10.23 ug/1 100 58) Fluoranthene 28.77 202 599924 10.17 ug/1 99 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. d 63) Pyrene 29.44 202 616475 10.98 ug/1 98 64) Butylbenzylphthalate 31.59 149 335242 10.34 ug/1 97 65) Benzo(a)anthracene 33.06 228 430657 10.22 ug/1 100 66) Bis(2-ethylhexyl)phthalate 33.38 149 454199 10.19 ug/1 100 67) Chrysene 33.19 228 419766 10.39 ug/1 99 69) Di-n-Octylphthalate 35.13 149 684964 9.67 ug/1 100 70) Benzo(b)fluoranthene 36.15 252 343117 9.43 ug/1 99

(#) = qualifier out of range (m) = manual integration CALIO.D NP091101.M Fri Oct 12 09:51:43 2001 Page 2

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