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GC/MS calibration data for TCLP method, Oct 2001

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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 11, 2001.

NYC-WTC_000087458–000087461

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C;\HPCHEM\1\DATA\OCT1101\CAL10.D Vial: 2 Acq On : 11 Oct 2001 10:24 am Operator: 209 GALOS Sample : mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 11 12:12 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth : NP091101 ■ -

Compound R.T. Qlon Response Cone Unit Qvalue 71) Benzo(k)fluoranthene 36.20 252 369054 10.76 ug/1 96 72) Benzo(a)pyrene 37.05 252 327215 IQjJLZ ug/1 98 73) Indeno(1,2,3-cd)pyrene 40.96 276 314237 IoTt? >ug/l 99 74) Dibenz(a,h)anthracene 41.03 278 254482 ug/1 99 75) Benzo(g,h,i)perylene 42.08 276 262013 .4 ug/1 99

(#) = qualifier out of range (m) = manual integration CALIO.D NP091101.M Fri Oct 12 09:51:44 2001 Page 3

NYC-WTC_000087460

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