GCMS reference results for sample AD28662, Dec 2001

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC0401\CAL80 .D Vial: 2 Acq On 4 Dec 2001 9:26 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 4 11:58 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.14 152 7908318 77.43 ug/1 99 3 4) Acenaphthene 20.71 153 5334105 73.04 ug/1 99 35) 2,4-Dinitrophenol 20.91 184 720820 90.62 ug/1 # 82 36) 4-Nitrophenol 21.21 65 800291 96.20 ug/1 89 37) 2,4-Dinitrotoluene 21.39 165 2145143 84.35 ug/1 # 91 38) Diethylphthalate 22.14 149 6047308 77.20 ug/1 99 39) 4-Chlorophenyl-phenylether 22.25 204 2275475 66.54 ug/1 96 40) Fluorene 22.23 166 5058001 67.49 ug/1 100 41) Azobenzen/ 1,2-Diphenylhyd 22.73 77 6508005 80.40 ug/L 96 43) 4,6-Dinitro-2-methylphenol 22.62 198 1161718 85.79 ug/1 95 44) N-Nitrosodiphenylamine 22.68 168 2598239 76.44 ug/1 94 45) 4-Bromophenyl-phenylether 23.70 248 1421598 75.48 ug/1 95 46) Hexachlorobenzene 24.14 284 . 1484278 71.67 ug/1 95 47) Pentachlorophenol 24.70 266 935030 95.44 ug/1 99 4 8) Phenanthrene 25.11 178 7020681 69.24 ug/1 98 49) Anthracene 25.24 178 7025756 69.52 ug/1 99 50) Di-n-butylphthalate 27.04 149 9489322 70.33 ug/1 99 51) Fluoranthene 28.72 202 7151998 73.07 ug/1 97 54) Pyrene 29.39 202 7209729 70.21 ug/1 93 55) Butylbenzylphthalate 31.54 149 3677766 68.57 ug/1 95 56) Benzo(a)anthracene 33.01 228 5322180 75.08 ug/1 99 57) Bis(2-ethylhexyl)phthalate 33.33 149 4479602 61.81 ug/1 99 58) Chrysene 33.15 228 5079258 73.06 ug/1 99 60) Di-n-Octylphthalate 35.07 149 7263284 66.09 ug/1 # 98 61) Benzo(b)fluoranthene 36.10 252 4808201 77.27 ug/1 99 62) Benzo(k)fluoranthene 36.10 252 4504082 70.53 ug/1 99 63) Benzo(a)pyrene 37.00 252 4222385 78.05 ug/1 98 64) Indeno(1,2,3-cd)pyrene 40.88 276 4564328 84.37 ug/1 100 65) Dibenz(a,h)anthracene 40.94 278 3568722 84.24 ug/1 97 66) Benzo(g,h,i)perylene 42.00 276 3886344m 84.08 ug/1

(#) = qualifier out of range (m) = manual integration CAL80.D NP112601.M Tue Dec 04 11:59:25 2001 Page 2

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