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GCMS calibration results for sample AD28263, Nov 2001

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Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.

NYC-WTC_000034168–000034174

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) t Data File C:\HPCHEM\1\DATA\NOV2701\CALIB40.D Vial: 2 Acq On 28 Nov 2001 12:49 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 15:07 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue NOV 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.12 152 5047719 39.40 ug/1 100 3 4) Acenaphthene 20.68 153 3560510 38.87 ug/1 100 35) 2,4-Dinitrophenol 20.89 184 335684 33.64 ug/1 99 36) 4-Nitrophenol 21.16 65 409013 39.20 ug/1 98 37) 2,4-Dinitrotoluene 21.35 165 1251958 39.25 ug/1 95 38) Diethylphthalate 22.11 149 3841080 39.09 ug/1 99 39) 4-Chlorophenyl-phenylether 22.23 204 1646299 38.38 ug/1 99 40) Fluorene 22.20 166 3584509 38.13 ug/1 99 41) Azobenzen/ 1,2-Diphenylhyd 22.70 77 3908499 38.50 ug/L 99 43) 4,6-Dinitro-2-methylphenol 22.56 198 596754 37.08 ug/1 94 44) N-Nitrosodiphenylamine 22.63 168 1686890 41.76 ug/1 99 45) 4-Bromophenyl-phenylether 23.69 248 868489 38.81 ug/1 99 46) Hexachlorobenzene 24.11 284 923771 37.53 ug/1 99 47) Pentachlorophenol 24.67 266 491152 42.19 ug/1 99 4 8) Phenanthrene 25.08 178 4567529 37.91 ug/1 99 49) Anthracene 25.21 178 4434583 36.92 ug/1 99 50) Di-n-butylphthalate 27.01 149 5893476 36.76 ug/1 100 51) Fluoranthene 28.6 202 4154665 35.72 ug/1 98 54) Pyrene 29.35 202 4163463 42.06 ug/1 98 55) Butylbenzylphthalate 31.52 149 1988783 38.47 ug/1 97 56) Benz o(a)anthracene 32.99 228 2635270 38.57 ug/1 99 57) Bis(2-ethylhexyl)phthalate 33.31 149 2416056 34.59 ug/1 99 58) Chrysene 33.12 228 2592900 38.69 ug/1 99 60) Di-n-Octylphthalate 35.05 149 3607464 37.38 ug/1 99 61) Benzo(b)fluoranthene 36.06 252 2140721 39.18 ug/1 98 62) Benzo(k)fluoranthene 36.13 252 2097134 37.39 ug/1 99 63) Benzo(a)pyrene 36.96 252 1832961 38.58 ug/1 99 64) Indeno(1,2,3-cd)pyrene 40.82 276 1970159 41.47 ug/1 99 65) Dibenz(a,h)anthracene 40.88 278 1563016 42.02 ug/1 100 66) Benzo (g, h, i) perylene 41.92 276 1650874 40.67 ug/1 98

(#) = qualifier out of range (m) = manual integration CALIB40.D GCMS1126.M Wed Nov 28 15:08:19 2001 Page 2

NYC-WTC_000034173

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