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← Document results/DEP Box 22/GCMS X 11/23/01 A 11/29/01
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GCMS calibration data for sample AD28593, Nov-Dec 2001

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Calibration results for gas chromatography-mass spectrometry analysis showing detector responses for standard compounds.

NYC-WTC_000034727–000034730

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\CALI25.D Vial: 3 Acq On : 29 Nov 2001 4:31 pm Operator: 209 GALOS Sample : calib 25 Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 14:50 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.11 152 2818424 25.33 ug/1 99 34) Acenaphthene 20.68 153 2013576 25.31 ug/1 100 35) 2,4-Dinitrophenol 20.88 184 107105 (1236 ug/1 91 36) 4-Nitrophenol 21.15 65 204793 22.60 ug/1 94 37) 2,4-Dinitrotoluene 21.34 165 668576 24.13 ug/1 96 38) Diethylphthalate 22.10 149 2147351 25.16 ug/1 99 39) 4-Chlorophenyl-phenylether 22.22 204 949379 25.48 ug/1 99 40) Fluorene 22.19 166 2055384 25.18 ug/1 100 41) Azobenzen/ 1,2-Diphenylhyd 22.69 77 2204595 25.00 ug/L 98 43) 4,6-Dinitro-2-methylphenol 22.55 198 256791 ( 18.60 ug/1 99 44) N-Nitrosodiphenylamine 22.62 168 916238 zb.43 ug/1 100 45) 4-Bromophenyl-phenylether 23.68 248 484770 25.24 ug/1 98 4 6) Hexachlorobenzene 24.10 284 520403 24.64 ug/1 98 47) Pentachlorophenol 24.67 266 216935 21.71 ug/1 99 48) Phenanthrene 25.06 178 2596002 25.11 ug/1 99 4 9) Anthracene 25.20 178 2576560 25.00 ug/1 99 50) Di-n-butylphthalate 27.01 149 3279920 23.84 ug/1 100 51) Fluoranthene 28.67 202 2351786 23.56 ug/1 96 54) Pyrene 29.34 202 2367947 26.87 ug/1 99 55) Butylbenzylphthalate 31.51 149 1061711 23.06 ug/1 93 56) Benzo(a)anthracene 32.98 228 1496286 24.59 ug/1 99 57) Bis(2-ethylhexyl)phthalate 33.31 149 1274810 20.49 ug/1 100 58) Chrysene 33.11 228 1449984 24.30 ug/1 99 60) Di-n-Octylphthalate 35.04 149 1788301 20.99 ug/1 # 97 61) Benzo(b)fluoranthene 36.05 252 1199228 24.86 ug/1 96 62) Benzo(k)fluoranthene 36.12 252 1276442 25.78 ug/1 99 63) Benzo(a)pyrene 36.94 252 1025558 24.45 ug/1 99 64) Indeno(l,2,3-cd)pyrene 40.80 276 1014319 24.19 ug/1 99 65) Dibenz(a,h)anthracene 40.86 278 811035 24.70 ug/1 99 66) Benzo (g, h, i)perylene 41.90 276 861653 24.05 ug/1 97

(#) = qualifier out of range (m) = manual integration CALI25.D GCMS1126.M Fri Nov 30 14:51:07 2001 Page 2

NYC-WTC_000034729

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NYC-WTC_000034729Source: NYC Law Department, mirrored locally

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