GCMS calibration data for sample AD28593, Nov-Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\CALI25.D Vial: 3 Acq On : 29 NOV 2001 4:31 pm Operator: 209 GALOS Sample : calib 25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 14:50 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 767415 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 2988169 20.00 ug/1 0.00 26) Acenaphthene-diO 20.57 164 1387791 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 1952442 20.00 ug/1 0.00 53) Chrysene-dl2 33.03 240 1021146 20.00 ug/1 0.00 59) Perylene-dl2 37.12 264 641195 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 29.91 235 11832 0.51 ug/mL -0.16 Spiked Amount 5.000 Recovery = 10.20% Target Compounds Qvalue 2) Pyridine 5.36 79 1348931m 24.69 ug/1 3) N-nitroso-dimethyl amine 5.42 74 840084 24.89 ug/1 98 4) Phenol 10.97 94 1685029 24.90 ug/1 98 5) bis(2-Chloroethyl)ether 11.14 93 1296360 24.47 ug/1 100 6) 2-Chlorophenol 11.24 128 1272130 24.86 Ug/1 98 7) 1,3-Dichlorobenzene 11.60 146 1391332 24.93 ug/1 100 8) 1,4-Dichlorobenzene 11.74 146 1405625 24.91 ug/1 99 9) 1,2-Dichlorobenzene 12.26 146 1292380 24.83 ug/1 98 10) 2-Methylphenol 12.55 108 1182529 25.54 ug/1 99 11) 2,2' -oxybis (1-Chloropropan 12.60 45 1732774 25.69 ug/1 98 12) 3&4-Methylphenpl 12.96 108 1204983 25.40 ug/1 100 13) N-Nitroso-di-n-propylamine 12.99 70 758060 25.12 ug/1 98 14) Hexachloroethane 13.08 117 517929 25.23 ug/1 96 16) Nitrobenzene 13.38 77 1158626 24.88 ug/1 99 17) Isophorone 14.03 82 2207828 24.60 ug/1 99 18) 2-Nitrophenol 14.29 139 686051 23.48 ug/1 97 19) 2,4-Dimethylphenol 14.45 107 1096006 25.00 ug/1 99 20) bis(2-Chloroethoxy)methane 14.72 93 1495393 24.81 ug/1 99 21) 2,4-Dichlorophenol 14.97 162 961854 24.88 ug/1 99 22) 1,2,4-Trichlorobenzene 15.19 180 1067356 24.60 ug/1 99 2 3) Naphthalene 15.36 128 3596896 25.19 ug/1 100 24) Hexachlorobutadiene 15.91 225 527327 24.94 ug/1 100 25) 4-Chloro-3-methylphenol 17.10 107 960204 24.87 ug/1 97 27) Hexachlorocyclopentadiene 18.09 237 165096 16.51 ug/1 99 28) 2,4,6-Trichlorophenol 18.36 196 593915 24.84 ug/1 99 29) 2,4,5-Trichlorophenol 18.47 196 641200 24.44 ug/1 100 30) 2-Chloronaphthalene 18.85 162 2015683 25.46 ug/1 99 31) Dimethylphthalate 19.96 163 2302504 24.97 ug/1 100 32) 2,6-Dinitrotoluene 20.17 165 534650m 24.53 ug/1 (#) = qualifier out of range (m) = manual integration CALI25.D GCMS1126.M Fri Nov 30 14:51:03 2001 Page 1

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