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GCMS calibration results for sample AD28263, Nov 2001

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Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.

NYC-WTC_000034168–000034174

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2601\CAL80 .D Vial: 6 Acq On : 26 Nov 2001 3:34 pm Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 12:44 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.13 152 7926258 78.11 ug/1 100 3 4) Acenaphthene 20.69 153 5515197 76.01 ug/1 99 35) 2,4-Dinitrophenol 20.90 184 751429 95.07 ug/1 97 36) 4-Nitrophenol 21.18 65 684344 82.80 ug/1 94 37) 2,4-Dinitrotoluene 21.36 165 2081883 82.39 ug/1 98 38) Diethylphthalate 22.12 149 6133461 78.80 ug/1 99 39) 4-Chlorophenyl-phenylether 22.24 204 2566255 75.52 ug/1 99 40) Fluorene 22.21 166 5556444 74.62 ug/1 100 41) Azobenzen/ 1,2-Diphenylhyd 22.71 77 6149318 76.46 ug/L 98 43) 4,6-Dinitro-2-methylphenol 22.59 198 1149772 85.96 ug/1 98 44) N-Nitrosodiphenylamine 22.65 168 2625369 78.19 ug/1 98 45) 4-Bromophenyl-phenylether 23.70 248 1435620 77.17 ug/1 98 46) Hexachlorobenzene 24.12 284 1553087 75.92 ug/1 98 47) Pentachlorophenol 24.68 266 909669 94.00 ug/1 98 4 8) Phenanthrene 25.09 178 7581188 75.69 ug/1 98 49) Anthracene 25.22 178 7598303 76.11 ug/1 99 50) Di-n-butylphthalate 27.02 149 10285011 77.17 ug/1 99 51) Fluoranthene 28.70 202 7454676 77.11 ug/1 100 54) Pyrene 29.37 202 7602760 78.62 ug/1 97 55) Butylbenzylphthalate 31.53 149 4106376 81.31 ug/1 96 56) Benzo(a)anthracene 33.00 228 5320781 79.71 ug/1 100 57) Bis(2-ethylhexyl)phthalate 33.32 149 5515098 80.81 ug/1 100 58) Chrysene 33.13 228 5097076 77.86 ug/1 99 60) Di-n-Octylphthalate 35.06 149 8692107 88.84 ug/1 100 61) Benzo(b)fluoranthene 36.08 252 4718589 85.18 ug/1 98 62) Benzo(k)fluoranthene 36.15 252 4497105 79.10 ug/1 100 63) Benzo(a)pyrene 36.98 252 3995112 82.96 ug/1 100 64) Indeno(l,2,3-cd)pyrene 40.85 276 4090034 84.93 ug/1 97 65) Dibenz(a,h)anthracene 40.92 278 3235663 85.80 ug/1 99 66) Benzo(g,h,i)perylene 41.96 276 3474615 84.44 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS1126.M Fri Nov 30 12:45:15 2001 Page 2

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