GCMS calibration results for sample AD28263, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2601\CAL80.D Vial: 6 Acq On : 26 NOV 2001 3:34 pm Operator: 209 GALOS Sample : calib mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 12:44 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 703520 20.00 ug/1 0.00 15) Naphthalene-d8 15.31 136 2705442 20.00 ug/1 0.00 26) Acenaphthene-diO 20.58 164 1265737 20.00 ug/1 0.00 42) Phenanthrene-diO 25.01 188 1891141 20.00 ug/1 0.02 53) Chrysene-dl2 33.04 240 1120346 20.00 ug/1 0.00 59) Perylene-dl2 37.13 264 736327 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 29.91 235 15376 0.68 ug/mL -0.16 Spiked Amount 5.000 Recovery = 13.60% Target Compounds Qvalue 2) Pyridine 5.35 79 4252029 84.90 ug/1 99 3) N-nitroso-dimethyl amine 5.45 74 2543725m 82.21 ug/1 4) Phenol 10.99 94 4788135 77.18 ug/1 91 5) bis(2-Chloroethyl)ether 11.15 93 3709653 76.39 ug/1 99 6) 2-Chlorophenol 11.25 128 3754174 80.03 ug/1 98 7) 1,3-Dichlorobenzene 11.61 146 4046784 79.10 ug/1 100 8) 1,4-Dichlorobenzene 11.75 146 4063536 78.54 ug/1 100 9) 1,2-Dichlorobenzene 12.26 146 3713525 77.83 ug/1 99 10) 2-Methylphenol 12.56 108 3310932 78.01 ug/1 100 11) 2,2' -oxybis (1-Chlor op ropan 12.60 45 4741400 76.67 ug/1 96 12) 3&4-Methylphenol 12.99 108 3323305 76.40 ug/1 99 13) N-Nitroso-di-n-propylamine 13.02 70 2168304 78.37 ug/1 99 14) Hexachloroethane 13.09 117 1499048 79.66 ug/1 97 16) Nitrobenzene 13.40 77 3302270 78.31 ug/1 99 17) Isophorone 14.06 82 6329928 77.91 ug/1 99 18) 2-Nitrophenol 14.30 139 2151277 81.33 ug/1 99 19) 2,4-Dimethylphenol 14.47 107 3034677 76.46 ug/1 100 20) bis(2-Chloroethoxy)methane 14.74 93 4200131 76.96 ug/1 99 21) 2,4-Dichlorophenol 14.98 162 2722407 77.76 ug/1 100 22) 1,2,4-Trichlorobenzene 15.20 180 3018586 76.84 ug/1 99 23) Naphthalene 15.38 128 9713149 75.13 ug/1 99 24) Hexachlorobutadiene 15.91 225 1472364 76.91 ug/1 99 25) 4-Chloro-3-methylphenol 17.11 107 2756866 78.86 ug/1 98 27) Hexachlorocyclopentadiene 18.09 237 825832 90.56 ug/1 98 28) 2,4,6-Trichlorophenol 18.37 196 1767933 81.06 ug/1 99 29) 2,4,5-Trichlorophenol 18 .48 196 1956205 81.75 ug/1 98 30) 2-Chloronaphthalene 18.87 162 5613775 77.74 ug/1 99 31) Dimethylphthalate 19.99 163 6581158 78.24 ug/1 100 32) 2,6-Dinitrotoluene 20.20 165 1617714m 81.39 ug/1 (#) = qualifier out of range (m) = manual integration CAL80.D GCMS1126.M Fri Nov 30 12:45:12 2001 Page 1

NYC-WTC_000034169