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GCMS reference analysis results for sample AD28593, Dec 2001

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Gas chromatography-mass spectrometry reference report listing concentrations of volatile organic compounds for sample AD28593.

NYC-WTC_000034722–000034726

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\1\DATA\NOV2 601\REFB.D Vial: 8 Acq On : 28 NOV 2001 12:07 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 17:57 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 20.11 152 426771 3.56 ug/1 99 3 4) Acenaphthene 20.67 153 313172 3.65 ug/1 98 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.32 65 2751 0.28 ug/1 # 1 37) 2,4-Dinitrotoluene 21.33 165 69516 2.33 ug/1 96 38) Diethylphthalate 22.08 149 354477 3.85 ug/1 99 39) 4-Chlorophenyl-phenylether 22.22 204 149475 3.72 ug/1 98 40) Fluorene 22.18 166 328826 3.74 ug/1 98 41) Azobenzen/ 1,2-Diphenylhyd 22.68 77 322675 3.39 ug/L 98 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 22.61 168 120986 3.44 ug/1 98 45) 4-Bromophenyl-phenylether 23.68 248 73679 3.78 ug/1 98 46) Hexachlorobenzene 24.09 284 76835 3.59 ug/1 96 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 425482 4.06 ug/1 98 49) Anthracene 25.19 178 384213 3.68 ug/1 100 50) Di-n-butylphthalate 27.00 149 510466 3.66 ug/1 99 51) Fluoranthene 28.67 202 364895 3.60 Ug/1 98 54) Pyrene 29.34 202 368935 4.31 ug/1 97 55) Butylbenzylphthalate 31.51 149 135647 3.03 ug/1 94 56) Benzo(a)anthracene 32.98 228 217262 3.67 ug/1 97 57) Bis(2-ethylhexyl)phthalate 33.31 149 166557 2.76 ug/1 99 58) Chrysene 33.10 228 246106 4.24 ug/1 99 60) Di-n-Octylphthalate 35.04 149 172531 2.01 ug/1 # 95 61) Benzo(b)fluoranthene 36.05 252 159538 3.28 ug/1 98 62) Benzo(k)fluoranthene 36.11 252 203708 4.09 ug/1 99 63) Benzo(a)pyrene 36.94 252 129850 3.07 ug/1 98 64) Indeno(l,2,3-cd)pyrene 40.80 276 141307 3.35 ug/1 98 65) Dibenz(a,h)anthracene 40.86 278 124994 3.78 ug/1 99 66) Benzo(g,h,i)perylene 41.87 276 134258 3.72 ug/1 100

(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Fri Nov 30 17:58:04 2001 Page 2

NYC-WTC_000034725

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NYC-WTC_000034725Source: NYC Law Department, mirrored locally

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