GCMS calibration results for sample AD28263, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) P Data File C:\HPCHEM\1\DATA\NOV2701\CALIB40 .D Vial: 2 Acq On 28 Nov 2001 12:49 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 15:07 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via DataAcq Meth : : Initial Calibration NP103001 37/18 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 899237 20.00 ug/1 0.00 15) Naphthalene-d8 15.31 136 3484195 20.00 ug/1 0.00 26) Acenaphthene-diO 20.58 164 1597853 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 2275209 20.00 ug/1 0.01 53) Chrysene-dl2 33.04 240 1146765 20.00 ug/1 0.00 59) Perylene-dl2 37.12 264 726347 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 30.07 235 200 0.01 ug/mL 0.00 Spiked Amount 5.000 Recovery = 0.20% Target Compounds Qvalue 2) Pyridine 5.36 79 2570931m 40.16 ug/1 3) N-nitroso-dimethyl amine 5.43 74 1581052 39.98 ug/1 100 4) Phenol 10.98 94 3029801 38.21 ug/1 90 5) bis(2-Chloroethyl)ether 11.14 93 2326967 37.49 ug/1 99 6) 2-Chlorophenol 11.24 128 2322527 38.73 ug/1 99 7) 1,3-Dichlorobenzene 11.60 146 2534986 38.76 ug/1 98 8) 1,4-Dichlorobenzene 11.75 146 2561605 38.73 ug/1 99 9) 1,2-Dichlorobenzene 12.26 146 2322889 38.09 ug/1 98 10) 2-Methylphenol 12.55 108 2093219 38.58 ug/1 100 11) 2,2'-oxybis(1-Chloropropan 12.60 45 3094699 39.15 ug/1 98 12) 3&4-Methylphenol 12.98 108 2118076 38.10 ug/1 99 13) N-Nitroso-di-n-propylamine 13.00 70 1377130 38.94 ug/1 98 14) Hexachloroethane 13.10 117 925841 38.49 ug/1 98 16) Nitrobenzene 13.39 77 2095279 38.58 ug/1 98 17) Isophorone 14.04 82 4037392 38.59 ug/1 99 18) 2-Nitrophenol 14.30 139 1316302 38.64 ug/1 98 19) 2,4-Dimethylphenol 14.45 107 1501160 29.37 ug/1 99 20) bis(2-Chloroethoxy)methane 14.72 93 2705825 38.50 ug/1 99 21) 2,4-Dichlorophenol 14.98 162 1768938 39.24 ug/1 100 22) 1,2,4-Trichlorobenzene 15.21 180 1929215 38.13 ug/1 99 23) Naphthalene 15.37 128 6330968 38.03 ug/1 100 24) Hexachlorobutadiene 15.91 225 945624 38.35 ug/1 100 25) 4-Chloro-3-methylphenol 17.11 107 1789788 39.76 ug/1 97 27) Hexachlorocyclopentadiene 18.09 237 438381 38.08 ug/1 99 28) 2,4,6-Trichlorophenol 18.36 196 1109522 40.30 ug/1 99 29) 2,4,5-Trichlorophenol 18.48 196 1233312 40.83 ug/1 98 30) 2-Chloronaphthalene 18.86 162 3582727 39.30 ug/1 99 31) Dimethylphthalate 19.97 163 4166249 39.23 ug/1 100 32) 2,6-Dinitrotoluene 20.18 165 1005164m 40.06 ug/1 (#) = qualifier out of range (m) = manual integration CALIB40.D GCMS1126.M Wed NOV 28 15:08:16 2001 Page 1

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