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GCMS reference analysis results for sample AD28263, Dec 2001

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Laboratory report of GCMS reference analysis for sample AD28263 conducted on November 30, 2001.

NYC-WTC_000034175–000034179

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C: \HPCHEM \ 1 \DATA\NOV2 6 01 \REFA. D Vial: 30 Acq On : 27 NOV 2001 5:17 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 15:18 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue

3 3) Acenaphthylene 20.10 152 256222 2.35 ug/1 99 3 4) Acenaphthene 20.66 153 196144 2.52 ug/1 99 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.33 65 1385 N.D. 37) 2,4-Dinitrotoluene 21.33 165 34410 1.27 ug/1 94 38) Diethylphthalate 22.08 149 236193 2.83 ug/1 99 39) 4-Chlorophenyl-phenylether 22.22 204 90364 2.48 ug/1 95 40) Fluorene 22 .18 166 207628 2.60 ug/1 99 41) Azobenzen/ 1,2-Diphenylhyd 22.68 77 201129 2.33 ug/L 98 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 22.61 168 83768 2.62 ug/1 99 45) 4-Bromophenyl-phenylether 23.67 248 42996 2.42 ug/1 94 46) Hexachlorobenzene 24.10 284 49348 2.53 ug/1 98 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 281403 2.95 ug/1 99 49) Anthracene 25.19 178 243159 2.55 ug/1 99 50) Di-n-butylphthalate 27.01 149 335841 2.64 ug/1 99 51) Fluoranthene 28.67 202 239855 2.60 ug/1 # 93 54) Pyrene 29.34 202 243498 3.02 ug/1 98 55) Butylbenzylphthalate 31.51 149 73349 1.74 ug/1 98 56) Benzo(a)anthracene 32.97 228 137722 2.47 ug/1 99 57) Bis(2-ethylhexyl)phthalate 33.31 149 123021 2.16 ug/1 98 58) Chrysene 33.09 228 172927 3.17 ug/1 100 60) Di-n-Octylphthalate 35.05 149 78671 0.97 ug/1 # 95 61) Benzo(b)fluoranthene 36.05 252 116608 2.55 ug/1 94 62) Benzo(k)fluoranthene 36.11 252 144219 3.07 ug/1 97 63) Benzo(a)pyrene 36.94 252 81841 2.06 ug/1 98 64) Indeno(1,2,3-cd)pyrene 40.80 276 87650 2.21 ug/1 97 65) Dibenz(a,h)anthracene 40.87 278 76860 2.47 ug/1 97 66) Benzo (g,h, i)perylene 41.90 276 85170 2.51 ug/1 96

(#) = qualifier out of range (m) = manual integration REFA.D NP112601.M Mon Dec 03 11:41:35 2001 Page 2

NYC-WTC_000034178

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