GCMS reference analysis results for sample AD28263, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2 601\REFA.D Vial: 30 Acq On : 27 NOV 2001 5:17 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 15:18 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.69 152 751669 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 2836295 20.00 ug/1 0.00 26) Ac enaphthene-dl0 20.57 164 1357161 20.00 ug/1 0.00 42) Phenanthrene-diO 25.00 188 1803477 20.00 ug/1 0.00 53) Chrysene-dl2 33.03 240 934943 20.00 ug/1 0.00 59) Perylene-dl2 37.11 264 607705 20.00 ug/1 0.00 System Monitoring Compounds 52) 2,4-DDD 30.07 235 63624 2.96 ug/mL 0.00 Spiked Amount 5.000 Recovery = 59.20% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.43 74 50035 1.51 ug/1 99 4) Phenol 11.13 94 5151 N.D. 5) bis(2-Chloroethyl)ether 11.13 93 129077 2.49 ug/1 97 6) 2-Chlorophenol 0.00 128 0 N.D. 7) 1,3-Dichlorobenzene 11.60 146 66285 1.21 ug/1 94 8) 1,4-Dichlorobenzene 11.60 146 66285 1.20 ug/1 93 9) 1,2-Dichlorobenzene 12.25 146 77577 1.52 ug/1 98 10) 2-Methylphenol 12.25 108 391 N.D. 11) 2,2' -oxybis (1-Chloropropan 12.59 45 177129 2.68 ug/1 # 92 12) 3&4-Methylphenol 0.00 108 0 N.D. 13) N-Nitroso-di-n-propylamine 12.98 70 75478 2.55 ug/1 99 14) Hexachloroethane 13.09 117 18155 0.90 ug/1 97 16) Nitrobenzene 13.37 77 97540 2.21 ug/1 96 17) Isophorone 14.03 82 228690 2.69 ug/1 98 18) 2-Nitrophenol 14.03 139 4636 N.D. 19) 2,4-Dimethylphenol 14.03 107 440 N.D. 20) bis(2-Chloroethoxy)methane 14.71 93 151591 2.65 ug/1 100 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 15.19 180 65426 1.59 ug/1 96 23) Naphthalene 15.36 128 300685 2.22 ug/1 99 24) Hexachlorobutadiene 15.91 225 18006 0.90 ug/1 91 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 2 7) Hexachlorocyclopentadiene 18.08 237 230 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 18.85 162 160292 2.07 ug/1 99 31) Dimethylphthalate 19.95 163 245264 2.72 ug/1 99 32) 2,6-Dinitrotoluene . 20.16 165 34619 1.62 ug/1 # 70 (#) = qualifier out of range (m) = manual integration REFA.D NP112601.M Mon Dec 03 11:41:32 2001 Page 1

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