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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/9/02
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GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000023099–000023106

Folder label: “GCMS X 5/8/02 A 5/9/02”

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Data File C:\HPCHEM\l\DATA\MAY0302\9572.D Vial: 46 Acq On 5 May 2002 12:06 pm Operator: Sample GC/MS SCAN 4/23 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.80 4.23 ug/1 384432 Naphthalene-d8 15.83 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 37 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1065 (14.796 min): 9572.D (-) m/z 73.10 100.00%! 73

5000 267 355 ----- 45 108125 154 177193 223 251 14.40 14.60 14.80 15.00 15.20 I |, »1 1 293 323339 h ’ ’’’’1’1 " i'' " i11" i" " i " " i ' । f 11 |i 11111 '1 ’ i1 ■' i “ 1 ■ i" " i" 11" 111 i m/z 267.05 33.23% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ' i ■ ■ .■M........... 14.40 14.60 14.80 15.00 15.20 m/Z 355.10 32.23% 191207 251 1 323339 ‘ 111'' I' 1′1′11111′111111 I ‘ "1 i ’ “ ■ I ' " I " " I " 1' 11 1 ‘ I " ' 11" " I'" ") " i “ " i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

14.40 14.60 14.80 15.00 15.20 5000 355 m/ z 356.10 11.19% 45

133149 223 193 - 340 370 281 ' I 1 1 " I ' 1 " I ’ ' 11 r 1 1 1 1 1 11 1 1 ITTI” I I 11 I I r-1 | I i" " I 11" " i1 ‘ " i" ■ " i "111"1' i " miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 9.19%

5000 267 179 356 45 147 . ..... .... 209 237 . .... ...... 312 341 11" " i' ' ' ।' " ' i" '111" 11"" i " " '' " i " 1' i " " i ■ " ' i'1 ■' r 1" i ■11111111 f1" 11"111 /z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9572.D GCMS0501.M Tue May 07 15:00:54 2002 Page 2

NYC-WTC_000023105

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