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GCMS calibration results, Feb-Mar 2002

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons on February 27, 2002.

NYC-WTC_000010394–000010396

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

4 Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB2502\REFB.D Vial: 31 Acq On : 26 Feb 2002 7:29 pm Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 14:17 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 18307 (1.73ug/1 # 88 31) 4-Bromophenyl-phenylether 24.37 248 13361 (1.95ug/1 92 32) Hexachlorobenzene 24.81 284 17225 (2.15ug/l 95 33) Phenanthrene 34) Anthracene 25.78 25.92 178 178 76517 60963 (2.34 ug/1 (1.90 ug/1 99 98 35) Di-n-butylphthalate 27.69 149 80507 1.76) ug/1 # 98 36) Fluoranthene 29.41 202 62745 C1.92uq/l # 90 3 9) Pyrene 30.09 202 66393 $2.32 ug/l # 92 40) Butylbenzylphthalate 32.21 149 16842 1.06ug/l # 92 41) Benzo(a)anthracene 33.73 228 38413 180 ug/l 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 23280 1.09 ug/1 96 43) Chrysene 33.85 228 50896 247/ug/1 97 45) Di-n-Octylphthalate 35.73 149 19331 0.58 ug/l # 95 46) Benzo(b)fluoranthene 36.85 252 34662 1.84 ug/1 97 47) Benzo(k)fluoranthene 36.85 252 31748 1.68 ug/1 96 4 8) Benzo(a)pyrene 37.85 252 20683 13% ug/1 # 93 49) Indeno(1,2,3-cd)pyrene 42.25 276 24633 173ug/1 93 5 0) Dibenz(a,h)anthracene 42.32 278 22014 2.02ug/l 94 51) Benzo(g,h,i)perylene 43.50 276 25376 2.21vug/l # 93

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0208.M Thu Feb 28 14:19:48 2002 Page 2

NYC-WTC_000010395

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NYC-WTC_000010395Source: NYC Law Department, mirrored locally

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