GCMS calibration results, Feb-Mar 2002

NYC 9/11 Public Portal Document

8 Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2502\REFB.D Vial: 31 Acq On : 26 Feb 2002 7:29 pm Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 14:17 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 / Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response 7’3Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.32 152 206023 20.00 ug/1 -0.03 10) Naphthalene-d8 15.96 136 781751 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 408428 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.71 188 540362 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 326515 20.00 ug/1 -0.06 44) Perylene-dl2 264 208326 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD g/m—0.30 Spiked Amount 5.000 60.80% )

olek Target Compounds Qvalue 2) N-nitroso-dimethyl amine ug/l # 75 3) bis(2-Chloroethyl)ether ) ug/1 91 4) 1,3-Dichlorobenzene 5W1 97 5) 1,4-Dichlorobenzene i>g/i 6) 1,2-Dichlorobenzene 58 ug/1 95 7) 2,2'-oxybi s(1-Chloroprop - 32ug/1 99 8) N-Nitroso-di-n-propylamine 13.59 70 1 87ug/l 87 9) Hexachloroethane 13.73 117 6123 .93^/1 96 11) Nitrobenzene 14.00 77 24664 53 ug/1 98 12) 1sophorone 14.65 82 52539 (1.93 ug/1 98 13) bis(2-Chloroethoxy)methane 15.33 93 35628 <0^719/1 97 14) 1,2,4-Trichlorobenzene 15.85 180 20559 1.54vug/l 94 15) Naphthalene 16.02 128 82766 1.99 ug/l 97 16) Hexachiorobutadiene 16.56 225 6302 (0.79ug/l 95 18) Hexachlorocyclopentadiene 18.76 237 603 N.D. 19) 2-Chloronaphthalene 19.53 162 43956 (1.81 uq/1 98 2 0) Dimethylphthalate 20.61 163 61831 2.12 ug/1 99 21) 2,6-Dinitrotoluene 20.83 165 7778 1.21 ug/1 95 2 2) Acenaphthylene 20.80 152 63096 1.79 ug/1 99 2 3) Acenaphthene 21.36 153 52870 .15 ug/1 98 24) 2,4-Dinitrotoluene 22.01 165 7390 0 91 ug/1 # 86 25) Diethylphthalate 22.75 149 58345 1.98 ug/l 95 26) 4-Chlorophenyl-phenylether 22.90 204 27024 .13ug/l 95 27) Fluorene 22.89 166 54622 Puq/l 98 28) Azobenzen/ 1,2-Diphenylhyd 23.37 77 48449 1.56 ug/L # 89

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0208.M Thu Feb 28 14:19:44 2002 Page 1

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